Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Concept Videos

Capillary Electrophoresis: Instrumentation01:20

Capillary Electrophoresis: Instrumentation

Capillary electrophoresis instrumentation typically consists of several key components. A high-voltage power supply generates the electric field necessary for the separation by connecting to an anode (the positively charged electrode) and a cathode (the negatively charged electrode) located in buffer reservoirs at each end of the capillary tube. The system includes a sample vial, a fused silica capillary tube coated with polyimide for mechanical strength through which the sample components...

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Identification of MNT fragments produced by an energy-degraded <math><mrow><mmultiscripts><mrow></mrow> <mrow></mrow> <mn>238</mn></mmultiscripts> <mtext>U</mtext></mrow></math> beam on a <math><mrow><mmultiscripts><mrow></mrow> <mrow></mrow> <mn>209</mn></mmultiscripts> <mtext>Bi</mtext></mrow></math> target at the FRS Ion Catcher.

The European physical journal. A, Hadrons and nuclei·2026
Same author

Excitation Spectra of the ^{12}C(p,d) Reaction near the η^{'}-Meson Emission Threshold Measured in Coincidence with High-Momentum Protons.

Physical review letters·2026
Same author

Progress and Perspectives in Poly(meth) Acrylate/Acrylamide Derived Biosensing Technologies.

Macromolecular rapid communications·2026
Same author

First Proton-Induced Cross Sections on a Stored Rare Ion Beam: Measurement of ^{118}Te(p,γ) for Explosive Nucleosynthesis.

Physical review letters·2025
Same author

Bound-State Beta Decay of ^{205}Tl^{81+} Ions and the LOREX Project.

Physical review letters·2024
Same author

A cross sectional study on molecular prevalence of Orientia tsutsugamushi in household rat population of South India.

Comparative immunology, microbiology and infectious diseases·2024

Related Experiment Video

Updated: May 8, 2026

A Sample Preparation Pipeline for Microcrystals at the VMXm Beamline
09:00

A Sample Preparation Pipeline for Microcrystals at the VMXm Beamline

Published on: June 17, 2021

Automated laboratory based X-ray beamline with multi-capillary sample chamber.

S Purushothaman1, B L L E Gauthé, N J Brooks

  • 1Department of Chemistry, Imperial College London, South Kensington Campus, London SW7 2AZ, United Kingdom.

The Review of Scientific Instruments
|September 7, 2013
PubMed
Summary

A new automated X-ray beamline enables high-throughput small-angle X-ray scattering (SAXS) analysis of up to 104 samples. This system allows precise temperature control for advanced materials research.

More Related Videos

Fully Autonomous Characterization and Data Collection from Crystals of Biological Macromolecules
07:11

Fully Autonomous Characterization and Data Collection from Crystals of Biological Macromolecules

Published on: March 22, 2019

Online Size-exclusion and Ion-exchange Chromatography on a SAXS Beamline
11:09

Online Size-exclusion and Ion-exchange Chromatography on a SAXS Beamline

Published on: January 5, 2017

Related Experiment Videos

Last Updated: May 8, 2026

A Sample Preparation Pipeline for Microcrystals at the VMXm Beamline
09:00

A Sample Preparation Pipeline for Microcrystals at the VMXm Beamline

Published on: June 17, 2021

Fully Autonomous Characterization and Data Collection from Crystals of Biological Macromolecules
07:11

Fully Autonomous Characterization and Data Collection from Crystals of Biological Macromolecules

Published on: March 22, 2019

Online Size-exclusion and Ion-exchange Chromatography on a SAXS Beamline
11:09

Online Size-exclusion and Ion-exchange Chromatography on a SAXS Beamline

Published on: January 5, 2017

Area of Science:

  • Materials Science
  • Biophysics
  • Analytical Chemistry

Background:

  • High-throughput analysis is crucial for understanding complex materials.
  • Precise temperature control is essential for studying phase transitions and material stability.

Purpose of the Study:

  • To develop an automated laboratory X-ray beamline for high-throughput small-angle X-ray scattering (SAXS) measurements.
  • To enable simultaneous temperature-controlled analysis of multiple samples.

Main Methods:

  • Development of an automated X-ray beamline with a multi-capillary sample chamber.
  • Integration of a rotating anode generator, 2D optoelectronic detector, and Franks X-ray optics.
  • Implementation of a custom LabVIEW framework for automated control and data acquisition.

Main Results:

  • The system can analyze up to 104 samples simultaneously.
  • Precise temperature control (±0.005 °C) is achieved for samples between 5 and 85 °C.
  • Typical exposure times are less than 5 minutes for lyotropic liquid crystalline samples.

Conclusions:

  • The developed automated beamline significantly enhances the efficiency of SAXS measurements.
  • The system facilitates detailed investigation of temperature-dependent properties of various materials.
  • This automation streamlines complex experimental workflows in materials science and related fields.