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A facile fabrication process for polystyrene nanoring arrays.

Zuzanna A Lewicka1, Arash Bahloul, William W Yu

  • 1Department of Chemistry, Rice University, Houston, TX 77005, USA. wyu6000@gmail.com colvin@rice.edu.

Nanoscale
|September 28, 2013
PubMed
Summary

Researchers created polystyrene nanoring arrays using simple methods like nanosphere lithography and plasma treatment. This process transformed nanospheres into graphitic nanorings, offering a new fabrication technique.

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Area of Science:

  • Materials Science
  • Nanotechnology
  • Surface Science

Background:

  • Polystyrene nanostructures are widely studied for various applications.
  • Developing cost-effective and scalable fabrication methods for nanostructures is crucial.
  • Understanding the transformation mechanisms of polymers under plasma treatment is essential.

Purpose of the Study:

  • To fabricate polystyrene nanoring arrays with controlled dimensions.
  • To investigate the effect of argon plasma treatment on polystyrene nanospheres.
  • To elucidate the mechanism behind polystyrene nanoring formation.

Main Methods:

  • Nanosphere lithography for initial nanosphere assembly.
  • Argon plasma treatment for nanostructure transformation.

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  • Organic solvent immersion and sonication for nanostructure development.
  • Scanning electron microscopy (SEM) for morphological analysis.
  • X-ray photoelectron spectroscopy (XPS) and Raman spectroscopy for compositional analysis.

    • Main Results:

    • Fabrication of polystyrene nanoring arrays with outer diameters from 130 to 230 nm.
    • Argon plasma treatment converted polystyrene nanospheres into hollow cone-shaped nanostructures.
    • Spectroscopic analysis revealed the formation of graphitic materials on the nanostructures due to plasma treatment.
    • A detailed mechanism for nanoring formation was proposed based on experimental observations.

    Conclusions:

    • A cost-effective and simple method for fabricating polystyrene nanoring arrays was successfully developed.
    • Argon plasma treatment plays a key role in transforming polystyrene nanospheres into graphitic nanostructures.
    • The study provides insights into the surface modification of polymers under plasma conditions and nanostructure formation.