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X-ray Diffraction of Biological Samples01:10

X-ray Diffraction of Biological Samples

X-ray diffraction or XRD is an analytical tool that utilizes X-rays to study ordered structures such as crystalline organic and inorganic samples, polycrystalline materials, proteins, carbohydrates, and drugs.
According to Bragg's law, when X-rays strike the sample positioned on a stage, the rays are  scattered by the electron clouds around the sample atoms. The  X-ray diffraction or scattering is caused by constructive interference of the X-ray waves that reflect off the internal crystal...

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Updated: May 7, 2026

Analysis of Contact Interfaces for Single GaN Nanowire Devices
11:13

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Published on: November 15, 2013

Structural investigation of GaInP nanowires using X-ray diffraction.

D Kriegner1, J M Persson, T Etzelstorfer

  • 1Institute of Semiconductor and Solid State Physics, Johannes Kepler University Linz, Altenbergerstr. 69, A-4040 Linz, Austria.

Thin Solid Films
|October 4, 2013
PubMed
Summary
This summary is machine-generated.

Investigating gallium indium phosphide (GaInP) nanowires reveals significant 20% variations in chemical composition. These findings highlight challenges in achieving uniform material properties for advanced electronic applications.

Keywords:
III–V semiconductorsNanowiresX-ray diffraction

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Area of Science:

  • Materials Science
  • Nanotechnology
  • Solid State Physics

Background:

  • Ternary III-V semiconductor nanowires like GaInP are crucial for advanced electronic and optoelectronic devices.
  • Achieving precise control over chemical composition and homogeneity in nanowire growth is essential for device performance.

Purpose of the Study:

  • To investigate the structural properties, chemical composition, and homogeneity of ternary gallium indium phosphide (GaInP) nanowires.
  • To understand the extent of compositional variations within samples and individual nanowires.

Main Methods:

  • Growth of GaInP nanowires using metal-organic vapor-phase epitaxy (MOVPE).
  • Analysis of X-ray diffraction (XRD) reciprocal space maps to study ensemble fluctuations.
  • Utilizing synchrotron X-ray sources with micro-beam capabilities to probe compositional gradients.
  • X-ray energy dispersive spectroscopy (XEDS) for compositional analysis within single nanowires.

Main Results:

  • XRD analysis revealed complex and varying material composition across the sample, with fluctuations up to 20%.
  • Synchrotron XRD measurements demonstrated compositional gradients along the sample length.
  • XEDS confirmed significant compositional variations within individual GaInP nanowires.

Conclusions:

  • The study highlights considerable challenges in achieving uniform chemical composition in MOVPE-grown GaInP nanowires.
  • Significant compositional inhomogeneity exists both across the sample and within individual nanowires.
  • These findings are critical for optimizing growth parameters and understanding limitations in GaInP nanowire-based technologies.