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Updated: May 7, 2026

Electrochemical Etching and Characterization of Sharp Field Emission Points for Electron Impact Ionization
Published on: July 12, 2016
Note: Automated electrochemical etching and polishing of silver scanning tunneling microscope tips
Stephen S Sasaki1, Shawn M Perdue, Alejandro Rodriguez Perez
1Department of Chemistry, University of California, Irvine, Irvine, California 92697, USA.
Abstract:
Fabrication of sharp and smooth Ag tips is crucial in optical scanning probe microscope experiments. To ensure reproducible tip profiles, the polishing process is fully automated using a closed-loop laminar flow system to deliver the electrolytic solution to moving electrodes mounted on a motorized translational stage. The repetitive translational motion is controlled precisely on the μm scale with a stepper motor and screw-thread mechanism. The automated setup allows reproducible control over the tip profile and improves smoothness and sharpness of tips (radius 27 ± 18 nm), as measured by ultrafast field emission.

