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Solid-phase Synthesis of [4.4] Spirocyclic Oximes
Published on: February 6, 2019
4-Phenyl-1,2,4-tri-aza-spiro-[4.5]dec-1-ene-3-thione
Mehmet Akkurt1, Joel T Mague, Shaaban K Mohamed
1Department of Physics, Faculty of Sciences, Erciyes University, 38039 Kayseri, Turkey.
Abstract:
In the title compound, C13H15N3S, the 4,5-di-hydro-3H-1,2,4-triazole ring is nearly planar [maximum deviation = 0.020 (1) Å], while the cyclo-hexane ring adopts a chair conformation. The dihedral angle between the 4,5-di-hydro-3H-1,2,4-triazole ring and the phenyl ring is 74.68 (7)°. No specific inter-molecular inter-actions are discerned in the crystal packing.
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