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High-pressure combinatorial process integrating hot isostatic pressing
Kenjiro Fujimoto1, Hiroki Morita, Yuji Goshima
1Department of Pure and Applied Chemistry, Faculty of Science and Technology, Tokyo University of Science , Yamazaki 2641, Noda, Chiba 278-8510, Japan.
Abstract:
A high-pressure combinatorial process integrating hot isostatic pressing (HIP) was developed by providing a reaction vessel with a high-pressure tightness based on a commercial flange. The reaction vessel can be used up to 200 MPa and 500 °C under HIP processing condition. Preparation of spinel-type MgAl2O4 from Mg(OH)2, Al(OH)3 and AlOOH was performed using the reaction vessel under 200 MPa and 500 °C as demonstration. The entire powder library was characterized using powder X-ray diffraction patterns, and the single phase of spinel-type MgAl2O4 was obtained from Mg(OH)2+Al(OH)3. These assessments corresponded with previously published data.
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