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Synthesis and Microdiffraction at Extreme Pressures and Temperatures
Published on: October 7, 2013
10.8K
Note: Compact optical fiber coupler for diamond anvil high pressure cells
1School of Physical Sciences, Ingram Building, University of Kent, Canterbury, Kent CT2 7NH, United Kingdom.
The Review of Scientific Instruments
|November 5, 2013
Summary
A new compact optical fiber coupler enables precise light transmission for high-pressure experiments in diamond anvil cells, even at low temperatures and in magnetic fields.
Area of Science:
- Optics and Photonics
- Materials Science
- High-Pressure Physics
Background:
- Diamond anvil cells (DACs) are crucial for high-pressure research but often have limited optical access.
- Integrating optical measurements within DACs, especially under extreme conditions (low temperature, high magnetic fields), presents significant challenges.
- Existing methods for optical interrogation of samples in DACs can be cumbersome or incompatible with certain experimental setups.
Purpose of the Study:
- To develop a compact and versatile optical fiber coupler for precise light delivery and collection within a diamond anvil high-pressure cell.
- To enable optical measurements in challenging environments, including low temperatures and high magnetic fields, where traditional optical access is limited.
- To demonstrate the utility of the coupler for in-situ pressure determination.
Main Methods:
- Development of a compact optical fiber coupler with integrated focusing optics and adjustments.
- Integration of the coupler with a diamond anvil cell for light transmission to and from the sample.
- Utilizing the coupler to perform ruby fluorescence spectroscopy for pressure measurement at cryogenic temperatures (1.2 K).
- Fabrication of the coupler using nonmagnetic beryllium copper for compatibility with high magnetic fields.
Main Results:
- The developed coupler allows precise focusing of light onto the sample within the DAC, despite its compact size.
- Successful demonstration of in-situ pressure measurement at 1.2 K using ruby fluorescence, showcasing the coupler's capability in low-temperature environments.
- The nonmagnetic construction facilitates its use in high magnetic fields, opening possibilities for combined high-pressure, low-temperature, and high-magnetic-field studies.
- The coupler is suitable for a broad range of optical measurements under high pressure.
Conclusions:
- A novel, compact optical fiber coupler significantly enhances the capabilities of diamond anvil cells for optical measurements.
- The coupler overcomes limitations of optical access in extreme experimental conditions, including low temperatures and high magnetic fields.
- This development is valuable for various scientific disciplines requiring in-situ optical characterization under high pressure.

