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Updated: Feb 9, 2026

Author Spotlight: A Rapid, Microwave-Assisted Hydrothermal Synthesis Of Nickel Hydroxide Nanosheets
Published on: August 18, 2023
Sponge-like nickel and nickel nitride structures for catalytic applications
Menny Shalom1, Valerio Molinari, Davide Esposito
1Max-Planck Institute of Colloids and Interfaces, Department of Colloid Chemistry, Research Campus Golm, 14424, Potsdam, Germany.
Researchers developed a safe, simple, and cost-effective method using molten inorganic salts to create high-surface-area nickel nitride and nickel-carbon-nitrogen materials for catalysis and energy applications.
Area of Science:
- Materials Science
- Catalysis
- Inorganic Chemistry
Background:
- Developing advanced materials with high surface area is crucial for catalytic applications.
- Existing synthesis methods for metal nitrides can be complex or hazardous.
- Nickel-based materials are promising for energy-related applications.
Purpose of the Study:
- To present a novel, safe, and simple method for fabricating air-stable nickel nitride and nickel embedded in a carbon and nitrogen matrix.
- To produce materials with high surface area suitable for catalytic applications.
- To explore the potential of molten inorganic salts as a reaction medium for synthesizing advanced materials.
Main Methods:
- Synthesis of nickel nitride and nickel-carbon-nitrogen matrix using molten inorganic salts.
- Characterization of the synthesized materials for their structure, composition, and surface properties.
- Evaluation of the materials' performance in catalytic applications.
Main Results:
- Successfully fabricated air-stable nickel nitride and nickel embedded in a carbon and nitrogen matrix.
- Achieved high surface area in the synthesized materials.
- Demonstrated the efficacy of molten inorganic salts as a reaction medium for safe and simple material synthesis.
Conclusions:
- The molten inorganic salt method provides a safe, simple, and cost-effective route for producing high-surface-area nickel-based materials.
- This approach opens new avenues for the synthesis of metal nitrides and metals for energy-related applications.
- The fabricated materials show promise for various catalytic applications.
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