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Laboratory test for ice adhesion strength using commercial instrumentation.

Chenyu Wang1, Wei Zhang, Adarsh Siva

  • 1Department of Chemical and Life Science Engineering, Virginia Commonwealth University , Richmond, Virginia 23284, United States.

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|December 26, 2013
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Summary

A new laboratory method uses a standard instrument to measure ice adhesion on surfaces. This approach simplifies ice release testing and aids in understanding surface properties affecting ice adhesion.

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Area of Science:

  • Materials Science
  • Surface Science
  • Tribology

Background:

  • Evaluating ice adhesion is crucial for various applications, including aerospace and infrastructure.
  • Existing laboratory methods often require specialized, custom-built equipment, limiting accessibility.
  • Understanding the fundamental mechanisms of ice adhesion to surfaces is an ongoing challenge.

Purpose of the Study:

  • To develop a novel, accessible laboratory test method for quantifying ice adhesion strength.
  • To validate the new method using a standard polymer, poly(methyl methacrylate) (PMMA).
  • To identify key experimental parameters influencing ice adhesion measurements.

Main Methods:

  • Utilized a commercially available dynamic mechanical analysis instrument (TA RSA-III) for ice adhesion testing.
  • Developed a method involving the removal of an ice cylinder from a polymer coating using a probe.
  • Measured the peak removal force (Ps) as a metric for ice adhesion strength.
  • Characterized PMMA coatings using Differential Scanning Calorimetry (DSC), Dielectric والكيمياء Analysis (DCA), and Tapping Mode Atomic Force Microscopy (TM-AFM).

Main Results:

  • Successfully established a laboratory ice adhesion test method without custom apparatus.
  • Identified the distance between the probe and the polymer surface as a critical variable affecting peak removal force (Ps).
  • Demonstrated the test's utility by measuring ice adhesion on poly(methyl methacrylate) (PMMA).

Conclusions:

  • The developed test method offers a readily available platform for studying ice adhesion.
  • This accessible method facilitates fundamental investigations into surface characteristics influencing ice adhesion.
  • The findings provide a foundation for developing improved anti-icing surfaces and materials.