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Ion Mobility-Mass Spectrometry Techniques for Determining the Structure and Mechanisms of Metal Ion Recognition and Redox Activity of Metal Binding Oligopeptides
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Presence of nickel in alpha-2 macroglobulin isolated from human serum by high performance liquid chromatography

S Nomoto1, F W Sunderman

  • 1Division of Clinical Chemistry, Shinshu University School of Medical Technology, Matsumoto, Japan.

Annals of Clinical and Laboratory Science
|January 1, 1988
PubMed

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Precipitation Gravimetry01:03

Precipitation Gravimetry

Precipitation gravimetry is based on converting an analyte into a sparingly soluble precipitate, which is separated by filtration and weighed. An ideal precipitate should be pure, insoluble, of known composition, and easily filtered from the reaction mixture.
In determining nickel by gravimetric analysis, a precipitant of ethanolic dimethylglyoxime is added to a hot nickel salt solution. This is quickly followed by the dropwise addition of dilute ammonia solution until precipitation occurs. A...