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Updated: Apr 30, 2026

A Simple Dewar/Cryostat for Thermally Equilibrating Samples at Known Temperatures for Accurate Cryogenic Luminescence Measurements
Published on: July 19, 2016
A cryogenic infrared calibration target
E J Wollack1, R E Kinzer1, S A Rinehart1
1NASA Goddard Space Flight Center, Greenbelt, Maryland 20771, USA.
Abstract:
A compact cryogenic calibration target is presented that has a peak diffuse reflectance, R ⩽ 0.003, from 800 to 4800 cm(-1) (12 - 2 μm). Upon expanding the spectral range under consideration to 400-10,000 cm(-1) (25 - 1 μm) the observed performance gracefully degrades to R ⩽ 0.02 at the band edges. In the implementation described, a high-thermal-conductivity metallic substrate is textured with a pyramidal tiling and subsequently coated with a thin lossy dielectric coating that enables high absorption and thermal uniformity across the target. The resulting target assembly is lightweight, has a low-geometric profile, and has survived repeated thermal cycling from room temperature to ∼4 K. Basic design considerations, governing equations, and test data for realizing the structure described are provided. The optical properties of selected absorptive materials-Acktar Fractal Black, Aeroglaze Z306, and Stycast 2850 FT epoxy loaded with stainless steel powder-are characterized and presented.
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