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Na1.67Mn2.17(MoO4)3.

Chahira Bouzidi1, Mohamed Faouzi Zid1, Ahmed Driss1

  • 1Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis ElManar, 2092 Manar II Tunis, Tunisia.

Acta Crystallographica. Section E, Structure Reports Online
|May 15, 2014
PubMed
Summary
This summary is machine-generated.

Disodium dimanganese tris-ortho-molybdate(VI) was synthesized and structurally characterized. Its framework features interconnected double-chains and channels hosting sodium cations, revealing a novel structure within the Ag2M2(MoO4)3 family.

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Area of Science:

  • Inorganic Chemistry
  • Solid-State Chemistry
  • Crystallography

Background:

  • Molybdates and manganese compounds are crucial in materials science.
  • Understanding complex inorganic structures aids in designing new materials.
  • The Ag2M2(MoO4)3 family exhibits diverse structural motifs.

Purpose of the Study:

  • To synthesize and characterize disodium dimanganese tris-[ortho-molybdate(VI)].
  • To elucidate the crystal structure and cation distribution.
  • To compare the structure with related inorganic phases.

Main Methods:

  • Solid-state reactions for synthesis.
  • X-ray diffraction for structural determination.
  • Cation site occupancy analysis.

Main Results:

  • The compound Na1.67Mn2.17(MoO4)3 was successfully synthesized.
  • A 3D framework structure with Mn2Mo2O14 double-chains and MoO4 tetrahedra was identified.
  • Channels within the framework accommodate Na+ cations with specific site occupancies, including a mixed Na/Mn site.

Conclusions:

  • The title compound is isotypic with the Ag2M2(MoO4)3 family.
  • The structural complexity arises from interconnected double-chains and tetrahedra.
  • Detailed structural analysis provides insights into cation interactions within inorganic frameworks.