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Related Experiment Videos

3,5-Dimethyl-2,6-di-phenyl-piperidine.

S Sathya1, K Prathebha1, G Usha1

  • 1PG and Research Department of Physics, Queen Mary's College, Chennai-4, Tamilnadu, India.

Acta Crystallographica. Section E, Structure Reports Online
|May 15, 2014
PubMed
Summary

This study details the molecular structure of a piperidine derivative, C19H23N, revealing specific substituent positions and phenyl ring orientation. Crystal analysis shows molecules form zigzag chains through C-H⋯π interactions.

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Area of Science:

  • Organic Chemistry
  • Crystallography
  • Molecular Structure

Background:

  • Piperidine derivatives are important scaffolds in medicinal chemistry.
  • Understanding molecular conformation and intermolecular interactions is crucial for drug design.

Purpose of the Study:

  • To elucidate the three-dimensional molecular structure of the title compound, C19H23N.
  • To investigate the conformational preferences of the piperidine and phenyl rings.
  • To characterize the crystal packing and intermolecular interactions.

Main Methods:

  • Single-crystal X-ray diffraction analysis was employed.
  • Conformational analysis of the piperidine ring was performed.
  • Intermolecular interactions were identified using C-H⋯π analysis.

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Main Results:

  • The piperidine ring adopts a chair conformation.
  • Phenyl rings are inclined at 52.76(16)°.
  • Methyl substituents are in axial and equatorial positions.
  • Molecules form zigzag chains via C-H⋯π interactions in the crystal.

Conclusions:

  • The study provides a detailed structural characterization of C19H23N.
  • The observed conformation and intermolecular interactions offer insights into structure-activity relationships.
  • This structural data can inform the design of related compounds.