Related Experiment Video
Updated: Apr 29, 2026

Syntheses, Crystallization, and Spectroscopic Characterization of 3,5-Lutidine N-Oxide Dehydrate
Published on: April 24, 2018
(E)-3-(Oxolan-2-yl-idene)-1-phenyl-pyrrolidine-2,5-dione
Ying Shao1, Yong-An Xia1, Zhu-Hong Wu1
1Key Laboratory of Fine Petrochemical Engineering, Changzhou University, Changzhou 213164, Jiangsu, People's Republic of China.
Abstract:
In the title compound, C14H13NO3, the dihedral angles between the central pyrrolidine ring and the pendant tetra-hydro-furan and phenyl rings are 5.34 (18) and 58.99 (17)°, respectively. The tetra-hydro-furan ring is almost planar (r.m.s. deviation = 0.008 Å). In the crystal, mol-ecules are linked by C-H⋯O inter-actions, generating a three-dimensional network.
Related Concept Videos
Structure and Nomenclature of Epoxides
Structure and Nomenclature of Alcohols and Phenols
Alcohols are one of the most important functional groups in organic chemistry. The name of alcohol comes from the hydrocarbon from which it is derived. Alcohols are organic molecules containing the functional hydroxyl or –OH group directly bonded to carbon. Phenols have an OH group directly attached to a benzene ring. While alcohols are colorless, phenol is a white crystalline compound with a characteristic "hospital smell" odor.
As with other organic compounds, alcohols and...
Preparation of Epoxides
Epoxides result from alkene oxidation, which can be achieved by a) air, b) peroxy acids, c) hypochlorous acids, and d) halohydrin cyclization.
Epoxidation with Peroxy Acids
Epoxidation of alkenes via oxidation with peroxy acids involves the conversion of a carbon–carbon double bond to an epoxide using the oxidizing agent meta-chloroperoxybenzoic acid, commonly known as MCPBA. Since the O–O bond of peroxy acids is very weak, the addition of electrophilic oxygen of peroxy...
Preparation of Diols and Pinacol Rearrangement
The reaction begins with transferring a proton from the acid catalyst to one of the hydroxyl groups, producing an oxonium ion.
Five-Membered Heterocyclic Aromatic Compounds: Overview
Hydrolysis of Chlorobenzene to Phenol: Dow Process

