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Updated: Apr 28, 2026

Synthesis and Catalytic Performance of Gold Intercalated in the Walls of Mesoporous Silica
Published on: July 9, 2015
Synthesis of mesoporous silica hollow nanospheres with multiple gold cores and catalytic activity
Junchen Chen1, Zhaoteng Xue1, Shanshan Feng1
1Department of Chemistry and Shanghai Key Laboratory of Molecular Catalysis and Innovative Materials, Laboratory of Advanced Materials, Fudan University, Shanghai 200433, PR China.
Abstract:
The core-shell Au@resorcinol-formaldehyde (RF) nanospheres with multiple cores have been successfully synthesized by a modified Stöber method. After coating mesoporous silica and the calcination, the Au@meso-SiO2 hollow nanospheres with multiple gold cores can be obtained, which have a high surface area (∼537 m(2)/g) and uniform pore size (∼2.5 nm). The Au@meso-SiO2 hollow nanospheres can be used as a catalyst for the reduction of 4-nitrophenol by NaBH4 into 4-aminophenol, and exhibit excellent catalytic performance.

