Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Experiment Videos

(E)-4-{[(Morpholin-4-yl)imino]-meth-yl}benzo-nitrile.

Zeliha Atioğlu1, Mehmet Akkurt2, Aliasghar Jarrahpour3

  • 1Ilke Education and Health Foundation, Cappadocia Vocational College, The Medical Imaging Techniques Program, 50420 Mustafapaşa, Ürgüp, Nevşehir, Turkey.

Acta Crystallographica. Section E, Structure Reports Online
|August 28, 2014
PubMed
Summary
This summary is machine-generated.

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Novel Benzotriazole-β-lactam Derivatives as Antimalarial Agents: Design, Synthesis, Biological Evaluation and Molecular Docking Studies.

Chemistry & biodiversity·2024
Same author

Crystal structure and Hirshfeld surface analysis of <i>N</i>-[(<i>Z</i>)-(2-hy-droxy-phen-yl)methyl-idene]aniline <i>N</i>-oxide.

Acta crystallographica. Section E, Crystallographic communications·2021
Same author

Crystal structure and Hirshfeld surface analysis of 5,7-diphenyl-1,2,3,5,6,7-hexa-hydro-imidazo[1,2-<i>a</i>]pyridine-6,6,8-tricarbo-nitrile methanol mono-solvate.

Acta crystallographica. Section E, Crystallographic communications·2021
Same author

Crystal structure and Hirshfeld surface analysis of 2-{[7-acetyl-4-cyano-6-hy-droxy-8-(4-meth-oxy-phen-yl)-1,6-dimethyl-5,6,7,8-tetra-hydro-iso-quino-lin-3-yl]sulfan-yl}-<i>N</i>-phenyl-acetamide.

Acta crystallographica. Section E, Crystallographic communications·2021
Same author

(3a<i>S</i>,4<i>R</i>,5<i>R</i>,6<i>S</i>,7a<i>R</i>)-4,5-Di-bromo-2-[4-(tri-fluoro-meth-yl)phen-yl]-2,3,3a,4,5,6,7,7a-octa-hydro-3a,6-ep-oxy-1<i>H</i>-isoindol-1-one: crystal structure and Hirshfeld surface analysis.

Acta crystallographica. Section E, Crystallographic communications·2021
Same author

Crystal structure and Hirshfeld surface analysis of 6-amino-8-phenyl-1,3,4,8-tetra-hydro-2<i>H</i>-pyrido[1,2-<i>a</i>]pyrimidine-7,9-dicarbo-nitrile.

Acta crystallographica. Section E, Crystallographic communications·2021

This study details the molecular structure of C12H13N3O, revealing a specific chair conformation of the morpholine ring and an E conformation of the N-N=C-C bridge. The crystal structure shows molecules stacking along the a axis without significant intermolecular interactions.

Area of Science:

  • Crystallography
  • Organic Chemistry
  • Molecular Structure

Background:

  • Understanding the three-dimensional arrangement of atoms in organic molecules is crucial for predicting their properties and reactivity.
  • Crystallographic studies provide precise details of molecular geometry and intermolecular interactions in the solid state.

Purpose of the Study:

  • To elucidate the crystal structure and molecular geometry of the title compound, C12H13N3O.
  • To analyze the conformation of the morpholine ring and the N-N=C-C bridge.
  • To investigate intermolecular interactions in the crystalline state.

Main Methods:

  • Single-crystal X-ray diffraction was employed to determine the molecular structure.
  • Analysis of bond lengths, bond angles, and torsion angles provided geometric details.
Keywords:
crystal structure

Related Experiment Videos

  • Crystal packing was examined to identify intermolecular forces.

    • Main Results:

    • The morpholine ring was found to adopt a chair conformation.
    • The mean plane of the morpholine ring is inclined at 16.78(12)° to the benzene ring.
    • The N-N=C-C bridge exhibits an E conformation with a torsion angle of 173.80(19)°.
    • Molecules were observed to stack along the a axis in the crystal lattice.
    • No significant intermolecular interactions were detected.

    Conclusions:

    • The study provides a detailed crystallographic description of C12H13N3O.
    • The observed conformations and packing arrangement offer insights into the solid-state behavior of this compound.