Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Concept Videos

Precipitate Formation and Particle Size Control01:16

Precipitate Formation and Particle Size Control

5.8K
In precipitation gravimetry, the precipitating agent should react specifically or selectively with the analyte. While a specific reagent reacts with the analyte alone, a selective reagent can react with a limited number of chemical species.
The obtained precipitate should be either a pure substance of known composition or easily converted to one by a simple process, such as ignition or drying. In addition, the precipitate should be insoluble and easily filterable. In general, filterability...
5.8K
Washing, Drying, and Ignition of Precipitates00:52

Washing, Drying, and Ignition of Precipitates

5.7K
After filtration, the precipitate is washed to remove coprecipitated impurities and any remaining mother liquor. Colloidal precipitates, such as silver chloride, are washed with an electrolyte (such as dilute nitric acid) to prevent the peptization of the precipitate. In the case of slightly soluble precipitates, the wash solution contains a common ion to reduce solubility. Lead sulfate, which is slightly soluble in water, is washed with dilute sulfuric acid. Similarly, wash solutions may be...
5.7K
Gravimetry: Inorganic And Organic Precipitating Agents00:49

Gravimetry: Inorganic And Organic Precipitating Agents

5.9K
In gravimetry, the precipitant is chosen carefully to obtain a pure solid that can be easily filtered. Common inorganic precipitants can be used to determine several cations and anions. In some cases, the formation of the same precipitate can be used to determine the cation and the anion. For example, the reaction of barium and chromate ions to give barium chromate is used to determine both barium and chromate. However, precipitates such as hydroxides, oxalates, and metal ammonium phosphates...
5.9K
Precipitation Processes01:12

Precipitation Processes

5.0K
The experimental conditions in a gravimetric analysis should be optimized to maximize the particle size and purity of the obtained precipitate. Ideally, the concentration of the precipitating reagent should be low with effective stirring to maintain low relative supersaturation for the growth of large crystals. In homogeneous precipitation, the precipitant is slowly generated by a chemical reaction in the solution to avoid local reagent excesses. For example, urea decomposes gradually to...
5.0K
Precipitation Gravimetry01:03

Precipitation Gravimetry

12.4K
Precipitation gravimetry is based on converting an analyte into a sparingly soluble precipitate, which is separated by filtration and weighed. An ideal precipitate should be pure, insoluble, of known composition, and easily filtered from the reaction mixture.
In determining nickel by gravimetric analysis, a precipitant of ethanolic dimethylglyoxime is added to a hot nickel salt solution. This is quickly followed by the dropwise addition of dilute ammonia solution until precipitation occurs. A...
12.4K
Recrystallization: Solid–Solution Equilibria01:10

Recrystallization: Solid–Solution Equilibria

4.1K
Recrystallization is a purification technique used to separate impurities from solid compounds. In this technique, no chemical reactions occur. Instead, it exploits physical properties only, specifically, the solubility differences between the desired compound and impurities, either at a single temperature or at different temperatures, and under other selected conditions. The solid-solution equilibrium (solubility equilibrium) of each component in the solution represents a binary phase...
4.1K

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Peridynamic study of the strength and failure of cemented cellular materials.

Physical review. E·2025
Same author

Particle fracture regimes from impact simulations.

Physical review. E·2024
Same author

Dynamic compaction of cohesive granular materials: scaling behavior and bonding structures.

Soft matter·2024
Same author

Contact networks and force transmission in aggregates of hexapod-shaped particles.

Soft matter·2024
Same author

From stress concentrations between inclusions to probability of breakage: A two-dimensional peridynamic study of particle-embedded materials.

Physical review. E·2023
Same author

An overlooked mechanism underlying the attenuated temperature response of soil heterotrophic respiration.

Journal of the Royal Society, Interface·2022

Related Experiment Video

Updated: Apr 21, 2026

Visually Based Characterization of the Incipient Particle Motion in Regular Substrates: From Laminar to Turbulent Conditions
11:51

Visually Based Characterization of the Incipient Particle Motion in Regular Substrates: From Laminar to Turbulent Conditions

Published on: February 22, 2018

8.2K

Initiation of immersed granular avalanches.

Patrick Mutabaruka1, Jean-Yves Delenne2, Kenichi Soga3

  • 1LMGC, UMR 5508, Université Montpellier 2, CNRS, Place E. Bataillon, 34095 Montpellier, France.

Physical Review. E, Statistical, Nonlinear, and Soft Matter Physics
|October 30, 2014
PubMed
Summary

Avalanches in immersed granular beds are triggered by vanishing dilatancy, with stability enhanced by negative pore pressure above a critical packing fraction.

More Related Videos

Visualization of Failure and the Associated Grain-Scale Mechanical Behavior of Granular Soils under Shear using Synchrotron X-Ray Micro-Tomography
09:00

Visualization of Failure and the Associated Grain-Scale Mechanical Behavior of Granular Soils under Shear using Synchrotron X-Ray Micro-Tomography

Published on: September 29, 2019

11.9K
Multi-electrode Array Recordings of Neuronal Avalanches in Organotypic Cultures
16:01

Multi-electrode Array Recordings of Neuronal Avalanches in Organotypic Cultures

Published on: August 1, 2011

27.7K

Related Experiment Videos

Last Updated: Apr 21, 2026

Visually Based Characterization of the Incipient Particle Motion in Regular Substrates: From Laminar to Turbulent Conditions
11:51

Visually Based Characterization of the Incipient Particle Motion in Regular Substrates: From Laminar to Turbulent Conditions

Published on: February 22, 2018

8.2K
Visualization of Failure and the Associated Grain-Scale Mechanical Behavior of Granular Soils under Shear using Synchrotron X-Ray Micro-Tomography
09:00

Visualization of Failure and the Associated Grain-Scale Mechanical Behavior of Granular Soils under Shear using Synchrotron X-Ray Micro-Tomography

Published on: September 29, 2019

11.9K
Multi-electrode Array Recordings of Neuronal Avalanches in Organotypic Cultures
16:01

Multi-electrode Array Recordings of Neuronal Avalanches in Organotypic Cultures

Published on: August 1, 2011

27.7K

Area of Science:

  • Physics
  • Geophysics
  • Material Science

Background:

  • Granular materials exhibit complex behaviors, especially when immersed in fluids.
  • Understanding avalanche initiation is crucial for geophysics and material handling.

Purpose of the Study:

  • To analyze avalanche initiation in fluid-immersed granular beds using simulations.
  • To investigate the role of packing fraction, pore pressure, and dilatancy.

Main Methods:

  • Coupled molecular dynamics-computational fluid dynamics (MD-CFD) simulations.
  • Analysis of shear strain, packing fraction, and pore pressures.
  • Exploration of granular microstructure and contact network anisotropy.

Main Results:

  • Bed stability increases with packing fraction (>0.59) due to negative excess pore pressure.
  • Avalanches initiate when dilatancy vanishes, independent of initial conditions.
  • Internal friction angle depends on inclination, not dilatancy, in fluid-immersed beds.

Conclusions:

  • Fluid-immersed granular material behavior is influenced by both hydrodynamics and microstructure.
  • Negative pore pressure and dilatancy play key roles in avalanche initiation and bed stability.
  • Contact network anisotropy explains the observed friction angle dependence on inclination.