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Updated: Apr 11, 2026

Evaluation of the Curing of Adhesive Systems by Rheological and Thermal Testing
Published on: July 3, 2020
Evaluation of the influence of three different temperatures on microleakage of two self-etch and one total-etch
Sahar Akbarian1, Farahnaz Sharafeddin2, Golsa Akbarian3
1Department of Operative Dentistry, Shiraz Dental School, Shiraz University of Medical Sciences, Shiraz, Iran.
Aim:
To evaluate the bonding temperature effect on dentin-restoration microleakage. The null hypothesis of the study is that the score of microleakage is identical among different adhesive bondings at different temperatures.
Materials And Methods:
Ninety caries free maxillary premolars were selected. Class V cavities were prepared on the cemento enamel junction (CEJ) of the buccal sides with enamel margins on occlusal sides and cementum margins on gingival sides. The specimens were divided into 3 groups: G1, single bond adhesive + Z250 composite; G2, P90 adhesive + Filtek Silorane composite; and G3, Clearfil SE bond + Clearfil APX. All groups were divided into three subgroups based on the adhesive temperature: A-4°C; B-25°C; and C-40°C. After coating the specimens with nail polish 1 mm beyond the margin of the restorations, they were stored in 0.5% basic Fuchsin dye solution for 24 hours. The teeth then were buccolingually sectioned and observed under a stereomicroscope.
Results:
There was no significant difference between microleakage of occlusal and gingival margins in each group. Clearfil SE bond and Adper single bond displayed lower microleakage than P90 adhesive at 4°C and 25°C. The most and least microleakage score for Adper single bond was at 40°C and 25°C respectively. Clearfil SE bond showed less microleakage at 25°C than 4°C and 40°C.
Conclusion:
Clearfil SE bond and Adper single bond displayed less microleakage at 25°C while there was no significant difference among for P90 adhesive microleakage at three temperatures.

