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The Extreme Conditions Beamline P02.2 and the Extreme Conditions Science Infrastructure at PETRA III
H P Liermann1, Z Konôpková1, W Morgenroth2
1Deutsches Elektronen-Synchrotron (DESY), Hamburg, Germany.
Journal of Synchrotron Radiation
|July 3, 2015
Summary
The Extreme Conditions Beamline P02.2 enables micro X-ray diffraction studies under simultaneous high pressure and temperature. It utilizes high-brilliance X-rays and fast detectors for time-resolved research.
Area of Science:
- Materials Science
- Condensed Matter Physics
- Geophysics
Background:
- High pressure and temperature studies are crucial for understanding material behavior under extreme conditions.
- Existing facilities may have limitations in simultaneous pressure-temperature control and resolution.
Purpose of the Study:
- To describe the Extreme Conditions Beamline P02.2 at PETRA III for advanced material research.
- To detail the beamline's capabilities, including X-ray optics, instrumental resolution, and sample environments.
- To highlight time-resolved studies under extreme conditions.
Main Methods:
- Micro X-ray diffraction (XRD) using a high-brilliance, high-energy X-ray source.
- Diamond anvil cell (DAC) for generating high pressures.
- Simultaneous high/low temperature control.
- Fast area detectors for time-resolved measurements.
Main Results:
- Detailed characterization of X-ray optics and instrumental resolution.
- Overview of diverse sample environments for DAC-based high-pressure research.
- Demonstration of time-resolved compression studies in the millisecond regime.
Conclusions:
- The Extreme Conditions Beamline P02.2 is a powerful facility for studying matter under extreme pressure and temperature.
- The beamline supports advanced, time-resolved research, advancing materials science and geophysics.
- The Extreme Conditions Science Infrastructure enhances high-pressure research capabilities at PETRA III.
Keywords:
PDFcryostatdiamond anvil cellextreme conditionshigh energieshigh-pressurehigh-temperaturelaser heatinglow temperaturemicro-diffractionradial diffractionresistive heatingtime-resolved diffraction
