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A 3D-printed Chamber for Organic Optoelectronic Device Degradation Testing
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Note: Small anaerobic chamber for optical spectroscopy.

Adrien A P Chauvet1, Rachna Agarwal2, William A Cramer2

  • 1Ecole Polytechnique Fédérale de Lausanne (EPFL), Laboratoire de Spectroscopie Ultrarapide, ISIC, Faculté des Sciences de Base, Station 6, 1015 Lausanne, Switzerland.

The Review of Scientific Instruments
|November 2, 2015
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Summary

Researchers developed a compact anaerobic chamber for analyzing oxygen-sensitive samples using spectroscopy. This novel chamber allows sample access and adjustment without compromising the hermetic environment, overcoming limitations of existing systems.

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Area of Science:

  • Biophysical chemistry
  • Spectroscopic analysis
  • Atmospheric control for biological samples

Background:

  • Studying oxygen-sensitive biological samples necessitates precise atmospheric control.
  • Existing commercial anaerobic chambers are often too large for compact spectroscopic systems.
  • Spectroscopic analysis requires unobstructed optical access through the chamber.

Purpose of the Study:

  • To design and present a novel, compact anaerobic chamber for spectroscopic analysis.
  • To overcome the limitations of current anaerobic chambers in terms of size and functionality.
  • To enable in-situ spectroscopic analysis of oxygen-sensitive samples.

Main Methods:

  • Development of a 1-liter anaerobic chamber.
  • Integration of a septum for sample access.
  • Design allowing sample manipulation while maintaining hermetic seal during spectroscopy.

Main Results:

  • A functional 1-liter anaerobic chamber suitable for broad-band spectroscopic analysis was created.
  • The chamber provides hermetic sealing and allows sample access via a septum.
  • The design permits adjustment of sample position without breaking the seal.

Conclusions:

  • The developed anaerobic chamber effectively addresses the need for controlled atmospheres in compact spectroscopic systems.
  • This innovation facilitates the study of oxygen-sensitive biological samples with enhanced experimental flexibility.
  • The chamber's design is suitable for various spectroscopic techniques requiring precise environmental control.