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Updated: Mar 28, 2026

Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples
Published on: June 19, 2018
An efficient plane-grating monochromator based on conical diffraction for continuous tuning in the entire soft X-ray
1X-ray Fluorescence Beamline, Elettra - Sincrotrone Trieste ScpA, SS 14, km 163.5 in Area Science Park, Basovizza, 34149 Trieste, Italy.
Reflection gratings in conical diffraction offer high efficiency for tender X-rays. This enables a tunable monochromator design with high throughput for X-ray spectroscopy applications.
Area of Science:
- X-ray optics
- Diffraction gratings
- Spectroscopy
Background:
- Reflection gratings with rectangular profiles exhibit high diffraction efficiency at grazing incidence for tender X-rays.
- Extreme off-plane (conical diffraction) orientation enhances grating performance.
Purpose of the Study:
- To explore the design of a conical diffraction monochromator for efficient and continuous tuning of photon energy.
- To evaluate the performance of such a monochromator for X-ray applications.
Main Methods:
- Utilizing reflection gratings in conical diffraction geometry.
- Employing a simple instrument design with a rotating plane grating and mirror.
- Incorporating a focusing mirror and exit slit for photon energy selection.
Main Results:
- The proposed monochromator scheme allows continuous tuning from below 1000 eV to 8 keV.
- High transmission is achieved as all components operate below the critical angle for total reflection.
- For tender X-rays (2-8 keV), the bandwidth is significantly larger than Si(111) double-crystal monochromators, offering higher flux.
- For soft X-rays (<1 keV), a relative spectral resolving power of approximately 10000 is achievable.
Conclusions:
- Conical diffraction monochromators offer a promising approach for high-throughput, tunable X-ray spectroscopy.
- The design provides flexibility in balancing flux and spectral bandwidth.
- This technology is suitable for both tender and soft X-ray energy ranges.
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