Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Experiment Video

Updated: Mar 28, 2026

Development of a 3D Graphene Electrode Dielectrophoretic Device
11:15

Development of a 3D Graphene Electrode Dielectrophoretic Device

Published on: June 22, 2014

12.6K

Robust Electrografting on Self-Organized 3D Graphene Electrodes.

Philippe Fortgang1, Teddy Tite2,3, Vincent Barnier4

  • 1Institut des Sciences Analytiques, UMR 5280, CNRS, Université de Lyon 1 , 5 rue de la Doua, 69100 Villeurbanne, France.

ACS Applied Materials & Interfaces
|December 30, 2015
PubMed
Summary

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Influence of the Rapid Thermal Nitriding Process on the Properties of TiN Thin Films Obtained from TiO<sub>2</sub> Sol-Gel Layers.

ACS omega·2026
Same author

Development of isoxazole-functionalized chitosan for enhanced anti-ulcer activity: From shrimp waste to therapeutic biopolymer.

International journal of biological macromolecules·2026
Same author

Hydrophilic interaction chromatography and tandem mass spectrometry for the characterization of methylated oligoribonucleotides.

Journal of pharmaceutical and biomedical analysis·2026
Same author

Surface activation and functionalization with aryl-diazonium chemistry enable biomolecules grafting on 3D printed carbon-based electrodes.

Bioelectrochemistry (Amsterdam, Netherlands)·2026
Same author

Antibacterial Properties of Low Silver Content ZrCu-Based PVD Thin Film Metallic Glasses: Effect of a Femtosecond Laser Texturing.

ACS applied materials & interfaces·2026
Same author

An anti-fouling multifunctional interface enables hierarchical validation and ultrasensitive electrochemical detection of Coxsackievirus A6 specific nucleic acids.

Bioelectrochemistry (Amsterdam, Netherlands)·2026

Researchers developed a novel 3D graphene electrode using pulsed laser deposition and a robust electrografting method for enhanced electrochemical sensing. This functionalized graphene electrode demonstrates excellent electron transfer and high redox probe loading for advanced applications.

Area of Science:

  • Electrochemistry
  • Materials Science
  • Nanotechnology

Background:

  • Developing high-performance electrodes is crucial for electrochemical applications.
  • Graphene-based electrodes offer unique properties but require improved fabrication and functionalization methods.

Purpose of the Study:

  • To report a self-organized 3D graphene electrode fabricated by pulsed laser deposition and thermal annealing.
  • To present a robust strategy for covalently attaching redox probes onto these 3D graphene electrodes.

Main Methods:

  • Fabrication of 3D graphene electrodes via pulsed laser deposition and thermal annealing.
  • Electrografting of an alkyne-terminated phenyl ring using diazonium salt chemistry.
  • Click chemistry (Cu(I)-catalyzed alkyne-azide cycloaddition) to attach a ferrocene redox probe.
Keywords:
X-ray photoelectron spectroscopyclick chemistrydiazonium electrograftingferroceneself-organized 3D graphene

More Related Videos

Fabrication of Three-Dimensional Graphene-Based Polyhedrons via Origami-Like Self-Folding
14:52

Fabrication of Three-Dimensional Graphene-Based Polyhedrons via Origami-Like Self-Folding

Published on: September 23, 2018

9.5K
Synthesis and Functionalization of 3D Nano-graphene Materials: Graphene Aerogels and Graphene Macro Assemblies
10:23

Synthesis and Functionalization of 3D Nano-graphene Materials: Graphene Aerogels and Graphene Macro Assemblies

Published on: November 5, 2015

14.6K

Related Experiment Videos

Last Updated: Mar 28, 2026

Development of a 3D Graphene Electrode Dielectrophoretic Device
11:15

Development of a 3D Graphene Electrode Dielectrophoretic Device

Published on: June 22, 2014

12.6K
Fabrication of Three-Dimensional Graphene-Based Polyhedrons via Origami-Like Self-Folding
14:52

Fabrication of Three-Dimensional Graphene-Based Polyhedrons via Origami-Like Self-Folding

Published on: September 23, 2018

9.5K
Synthesis and Functionalization of 3D Nano-graphene Materials: Graphene Aerogels and Graphene Macro Assemblies
10:23

Synthesis and Functionalization of 3D Nano-graphene Materials: Graphene Aerogels and Graphene Macro Assemblies

Published on: November 5, 2015

14.6K

Main Results:

  • The 3D graphene electrode exhibited excellent electron transfer kinetics.
  • A dense grafting of ferrocene derivatives was achieved with a surface coverage of 4.9 × 10⁻¹⁰ mol cm⁻².
  • The functionalized electrode showed a stable signal for over 22 days, with multilayer grafting enabling higher probe loading.

Conclusions:

  • The developed self-organized 3D graphene electrode and functionalization strategy are highly promising for electrochemical sensing.
  • This approach facilitates the creation of advanced graphene-based sensors with tailored functionalities.