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Phase Engineering of 2D Tin Sulfides.

Zafer Mutlu1, Ryan J Wu2, Darshana Wickramaratne3

  • 1Materials Science and Engineering Program, University of California, Riverside, CA, 92525, USA.

Small (Weinheim an Der Bergstrasse, Germany)
|April 22, 2016
PubMed
Summary

This study demonstrates phase-selective growth of tin disulfide (SnS2) and tin(II) sulfide (SnS) crystals. Controlled synthesis of these 2D tin sulfides is crucial for their electronic and optical applications.

Keywords:
2D materialsSnSSnS2phase engineeringtin sulfides

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Area of Science:

  • Materials Science
  • Solid State Chemistry
  • Nanotechnology

Background:

  • Tin sulfides exhibit diverse electronic and optical properties due to various phases and polytypes.
  • Layered 2D structures of tin sulfides are key to their unique characteristics.
  • Controlling phase, polytype, and thickness is essential for harnessing tin sulfide properties.

Purpose of the Study:

  • To achieve phase-selective growth of hexagonal tin (IV) sulfide (SnS2) and orthorhombic tin (II) sulfide (SnS) crystals.
  • To develop a method for synthesizing large-area (over tens of microns) tin sulfide crystals.
  • To characterize the synthesized tin sulfide phases and validate findings with theoretical calculations.

Main Methods:

  • Atmospheric pressure vapor-phase deposition using tin (IV) oxide (SnO2) and sulfur (S) powders.
  • Growth of tin sulfide crystals on silicon dioxide (SiO2) substrates in a horizontal quartz tube furnace.
  • Characterization using microscopy, spectroscopy, and ab initio density functional theory (DFT) calculations.

Main Results:

  • Successful phase-selective growth of hexagonal SnS2 and orthorhombic SnS crystals.
  • Crystals achieved diameters exceeding tens of microns.
  • Experimental results were consistent with DFT calculations, confirming phase and structure.

Conclusions:

  • The atmospheric pressure vapor-phase method enables controlled synthesis of distinct tin sulfide phases.
  • This controlled growth is vital for tailoring the electronic and optical properties of 2D tin sulfides.
  • The study provides a foundation for utilizing SnS2 and SnS in advanced material applications.