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Real-time microstructure imaging by Laue microdiffraction: A sample application in laser 3D printed Ni-based

Guangni Zhou1, Wenxin Zhu1, Hao Shen1

  • 1Center for Advancing Materials Performance from the Nanoscale (CAMP-Nano), State Key Laboratory for Mechanical Behavior of Materials, Xi'an Jiaotong University, Xi'an, Shaanxi 710049, P.R. China.

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Summary

A new method visualizes microstructural features from Laue microdiffraction data in real time. This approach simplifies analysis for researchers without advanced computing, enabling faster material characterization.

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Area of Science:

  • Materials Science
  • Crystallography
  • X-ray Diffraction

Background:

  • Synchrotron-based Laue microdiffraction analyzes crystal structure, orientation, and defects in polycrystalline solids.
  • Standard analysis of numerous Laue patterns is computationally intensive, limiting accessibility.

Purpose of the Study:

  • To develop a novel, accessible data analysis approach for Laue microdiffraction.
  • To enable real-time visualization of microstructural features during experiments.

Main Methods:

  • Plotting distributions of average recorded and filtered Laue pattern intensities.
  • Applying the method to a laser-assisted 3D printed Ni-based superalloy.

Main Results:

  • Real-time visualization of microstructural features like microcracks and carbides.
  • Successful imaging of features in a Ni-based superalloy significantly faster than data collection.

Conclusions:

  • The developed analytical approach is broadly applicable to various crystalline solids.
  • Extends Laue microdiffraction utility for time-critical experiments and real-time decision-making.