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Updated: Mar 14, 2026

Fizzy Extraction of Volatile Organic Compounds Combined with Atmospheric Pressure Chemical Ionization Quadrupole Mass Spectrometry
Published on: July 14, 2017
Fast analysis of volatile compounds from Lippia citriodora with nanoporous aluminum wire as solid-phase
Mohammad Nemati Kharajuo1, Marzieh Piryaei2, Marzieh Babashpour Asl1
1a Department of Horticulture, College of Agriculture , Islamic Azad University , Maragheh , Iran.
Abstract:
In this study, the efficiency of nanoporous aluminium wires as fibres for headspace solid-phase microextraction (HS-SPME) of volatile compounds from Lippia citriodora was investigated and compared with two anodised methods. The prepared fibres are durable with very good chemical and thermal stability which can be coupled to GC and GC/MS. A one at-a-time optimisation strategy was applied for optimising the important extraction parameters such as extraction temperature, extraction time, sample mass and added water. Compared with hydrodistillation (HD), HS-SPME provide the advantages of a small amount of sample, time-saving, simplicity and cheapness.
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