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Updated: May 5, 2026

Characterization of Ultra-fine Grained and Nanocrystalline Materials Using Transmission Kikuchi Diffraction
Published on: April 1, 2017
Dynamic creation and evolution of gradient nanostructure in single-crystal metallic microcubes
Ramathasan Thevamaran1, Olawale Lawal2, Sadegh Yazdi2
1Department of Materials Science and NanoEngineering, Rice University, Houston, TX 77005, USA. thevamaranr@rice.edu elt@rice.edu.
High-velocity impacts dynamically create extreme gradient nanograined structures in silver microcubes. These transformations offer new pathways for developing advanced metals with high strength and toughness for aerospace applications.
Area of Science:
- Materials Science
- Nanotechnology
- Mechanical Engineering
Background:
- Single-crystal silver microcubes are synthesized using a bottom-up seed-growth method.
- Understanding material behavior under extreme conditions is crucial for advanced engineering.
Purpose of the Study:
- To investigate the dynamic creation and static evolution of extreme gradient nanograined structures.
- To explore deformation mechanisms in silver microcubes subjected to high-velocity impacts.
Main Methods:
- Synthesized near-defect-free single-crystal silver microcubes.
- Utilized laser-induced projectile impact testing to launch microcubes at supersonic velocities (~400 m/s).
- Analyzed nanostructural transformations resulting from impacts against an impenetrable substrate.
Main Results:
- Demonstrated dynamic formation and static evolution of extreme gradient nanograined structures.
- Observed significant nanostructural transformations driven by high strain rates, strain gradients, and recrystallization.
- Revealed insights into deformation mechanisms influenced by crystal and sample-shape symmetries.
Conclusions:
- High-velocity impacts are effective in creating gradient nanograined structures in metals.
- These nanostructural transformations show potential for developing high-strength, high-toughness metals.
- The findings support applications in aerospace components requiring superior material properties.
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