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A compact and versatile dynamic flow cryostat for photon science.

Peter J E M van der Linden1, Marco Moretti Sala1, Christian Henriquet1

  • 1ESRF-The European Synchrotron, CS40220, 38043 Grenoble Cedex 9, France.

The Review of Scientific Instruments
|December 3, 2016
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Summary
This summary is machine-generated.

A new helium gas flow cryostat offers efficient sample cooling for X-ray experiments. This compact, versatile cryostat enables rapid sample changes and operates across a wide temperature range, enhancing synchrotron-based research.

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Area of Science:

  • Materials Science and Engineering
  • Condensed Matter Physics
  • Analytical Chemistry

Background:

  • Synchrotron X-ray techniques require precise sample environments for optimal data acquisition.
  • Efficient and stable temperature control is crucial for various X-ray scattering and spectroscopy methods.
  • Existing cryostats may present limitations in terms of sample changing speed, temperature range, or operational flexibility.

Purpose of the Study:

  • To introduce a novel helium gas flow cryostat designed for synchrotron X-ray beamlines.
  • To demonstrate the cryostat's capability for efficient sample cooling and rapid sample manipulation.
  • To highlight its adaptability for diverse X-ray techniques and operational conditions.

Main Methods:

  • Development of a compact helium gas flow cryostat with direct sample immersion in the cooling flow.
  • Integration of a removable sample holder for quick sample exchange (under 5 minutes).
  • Characterization of temperature range (2.5-325 K) and stability (better than 0.1 K).

Main Results:

  • Achieved highly efficient sample cooling due to direct contact with helium flow.
  • Demonstrated rapid sample changes at any operational temperature.
  • Confirmed wide optical access and omnidirectional operability for versatile X-ray experiments.

Conclusions:

  • The developed helium gas flow cryostat provides an efficient, user-friendly solution for synchrotron X-ray experiments.
  • Its performance characteristics make it suitable for a broad range of techniques including inelastic X-ray scattering, powder diffraction, and X-ray absorption spectroscopy.
  • The cryostat has been successfully implemented across multiple synchrotron facilities (ESRF, ALBA, DLS).