A sub-ms pressure jump setup for time-resolved X-ray scattering

We present a new experimental setup for time-resolved solution small-angle X-ray scattering (SAXS) studies of kinetic processes induced by sub-ms hydrostatic pressure jumps. It is based on a high-force piezo-stack actuator, with which the volume of the sample can be dynamically compressed. The presented setup has been designed and optimized for SAXS experiments with absolute pressures of up to 1000 bars, using transparent diamond windows and an easy-to-change sample capillary. The pressure in the cell can be changed in less than 1 ms, which is about an order of magnitude faster jump than previously obtained by dynamic pressure setups for SAXS. An additional temperature control offers the possibility for automated mapping of p-T phase diagrams. Here we present the technical specifications and first experimental data taken together with a preview of new research opportunities enabled by this setup.