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Updated: Mar 9, 2026

A Sample Preparation Pipeline for Microcrystals at the VMXm Beamline
Published on: June 17, 2021
Systematic search for spherical crystal X-ray microscopes matching 1-25 keV spectral line sources
Marius S Schollmeier1, Guillaume P Loisel1
1Sandia National Laboratories, Albuquerque, New Mexico 87185, USA.
Abstract:
Spherical-crystal microscopes are used as high-resolution imaging devices for monochromatic x-ray radiography or for imaging the source itself. Crystals and Miller indices (hkl) have to be matched such that the resulting lattice spacing d is close to half the spectral wavelength used for imaging, to fulfill the Bragg equation with a Bragg angle near 90∘ which reduces astigmatism. Only a few suitable crystal and spectral-line combinations have been identified for applications in the literature, suggesting that x-ray imaging using spherical crystals is constrained to a few chance matches. In this article, after performing a systematic, automated search over more than 9 × 106 possible combinations for x-ray energies between 1 and 25 keV, for six crystals with arbitrary Miller-index combinations hkl between 0 and 20, we show that a matching, efficient crystal and spectral-line pair can be found for almost every Heα or Kα x-ray source for the elements Ne to Sn. Using the data presented here it should be possible to find a suitable imaging combination using an x-ray source that is specifically selected for a particular purpose, instead of relying on the limited number of existing crystal imaging systems that have been identified to date.
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