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Updated: Mar 8, 2026

High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy
Published on: October 9, 2020
Magnetic resonance spectroscopy of an atomically thin material using a single-spin qubit
I Lovchinsky1, J D Sanchez-Yamagishi1,2, E K Urbach1
1Department of Physics, Harvard University, Cambridge, MA 02138, USA.
Researchers developed a new nanometer-scale nuclear quadrupole resonance (NQR) spectroscopy technique. This method uses diamond impurities to probe 2D materials like hexagonal boron nitride (h-BN) at the atomic level.
Area of Science:
- Condensed Matter Physics
- Quantum Information Science
- Materials Science
Background:
- Two-dimensional (2D) materials are crucial for novel phenomena and technologies.
- Probing atomic-scale materials is challenging for traditional macroscopic techniques.
- Existing methods struggle to interface with the reduced dimensionality of 2D materials.
Purpose of the Study:
- To demonstrate a novel method for probing 2D material properties at the nanoscale.
- To overcome limitations of traditional measurement techniques for atomic-scale materials.
- To enable the characterization of low-dimensional nanoscale materials.
Main Methods:
- Utilized nanometer-scale nuclear quadrupole resonance (NQR) spectroscopy.
- Employed individual atomlike impurities in diamond as probes.
- Leveraged coherent manipulation of nitrogen-vacancy (NV) color centers in diamond.
Main Results:
- Successfully probed nanoscale ensembles of atomically thin hexagonal boron nitride (h-BN).
- Achieved sensitivity down to approximately 30 nuclear spins.
- Demonstrated a viable technique for nanoscale characterization of 2D materials.
Conclusions:
- This NQR spectroscopy method provides unprecedented nanoscale insight into 2D materials.
- The technique facilitates the development of new quantum hybrid systems.
- Coherent coupling between atomlike systems and 2D materials is now feasible.
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