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Rotary shear experiments under X-ray micro-computed tomography.

Qi Zhao1, Nicola Tisato2, Giovanni Grasselli1

  • 1Department of Civil Engineering, University of Toronto, 35 St. George Street, Toronto, Ontario M5S 1A4, Canada.

The Review of Scientific Instruments
|February 3, 2017
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Summary
This summary is machine-generated.

A new rotary shear apparatus (ERDμ-T) combined with X-ray micro-computed tomography (μCT) allows real-time observation of material deformation. This innovation links physical parameters to internal structural changes during frictional sliding.

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Area of Science:

  • Materials Science
  • Mechanical Engineering
  • Tribology

Background:

  • Understanding frictional behavior and material deformation under shear stress is crucial for engineering applications.
  • In situ and in operando observation methods are needed to capture dynamic processes without perturbing experimental conditions.

Purpose of the Study:

  • To design, assemble, and calibrate a novel rotary shear apparatus (ERDμ-T) integrated with X-ray micro-computed tomography (μCT).
  • To demonstrate the capability of the ERDμ-T system for studying the frictional behavior and deformation of materials under shear stress.

Main Methods:

  • Development and calibration of the ERDμ-T apparatus for precise measurement of normal force, torque, sample shortening, and shearing velocity.
  • Integration of X-ray micro-computed tomography (μCT) for in situ and in operando visualization of internal specimen deformation during shearing.
  • Performing shear experiments on an aluminum alloy sample at incremental steps.

Main Results:

  • Successful demonstration of the ERDμ-T apparatus's capability to study frictional behavior.
  • Acquisition of μCT imagery synchronized with physical measurements, providing a comprehensive understanding of deformation processes.
  • Observation of how rough surfaces interact and deform under controlled pressure and temperature.

Conclusions:

  • The ERDμ-T system effectively links variations in physical parameters to the evolution of internal material structures.
  • The combined apparatus provides novel insights into fracturing and frictional sliding mechanisms in solid materials.
  • This technology enables non-perturbative, real-time analysis of material deformation during shear testing.