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Improving microstructural quantification in FIB/SEM nanotomography.

Joshua A Taillon1, Christopher Pellegrinelli2, Yi-Lin Huang2

  • 1University of Maryland, Materials Science and Engineering, College Park, MD 20742, United States.

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|August 26, 2017
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Summary
This summary is machine-generated.

Focused Ion Beam/Scanning Electron Microscopy nanotomography (FIB-nt) improves 3D microstructure analysis. New techniques enhance data quality and enable advanced quantification for materials engineering applications.

Keywords:
3D reconstructionFocused ion beamMicrostructure quantificationScanning electron microscopyTortuosityTriple phase boundaries

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Area of Science:

  • Materials Science
  • Nanotechnology
  • Microscopy

Background:

  • Three-dimensional microstructure dictates material performance and device engineering.
  • Focused Ion Beam/Scanning Electron Microscopy nanotomography (FIB-nt) is key for subsurface feature analysis.
  • Advanced FIB-nt analysis remains challenging in data acquisition and post-processing.

Purpose of the Study:

  • To present techniques for improving FIB-nt data quality.
  • To introduce methods for advanced microstructural quantification.
  • To demonstrate practical implementation using a solid oxide fuel cell cathode.

Main Methods:

  • Data acquisition optimization for FIB-nt.
  • Post-processing strategies for enhanced nanotomographic analysis.
  • Application of techniques to a solid oxide fuel cell cathode.

Main Results:

  • Improved quality of acquired 3D microstructural data.
  • Successful implementation of advanced microstructural quantifications.
  • Demonstrated adaptability of methodologies across material systems.

Conclusions:

  • Developed techniques enhance the utility of FIB-nt for materials analysis.
  • Methodologies are applicable beyond the studied solid oxide fuel cell cathode.
  • Advanced microstructural quantification is made more accessible through these methods.