Related Experiment Video
Updated: Feb 18, 2026

08:58
Processing of Bulk Nanocrystalline Metals at the US Army Research Laboratory
Published on: March 7, 2018
9.8K
Wear Behavior and Microstructure of Mg-Sn Alloy Processed by Equal Channel Angular Extrusion
Jung-Hsuan Chen1, Yen-Chen Shen2, Chuen-Guang Chao3
1Department of Industrial Education, National Taiwan Normal University, Taipei 106, Taiwan. jhchen@ntnu.edu.tw.
Materials (Basel, Switzerland)
|November 17, 2017
Summary
Equal Channel Angular Extrusion (ECAE) refines Mg-Sn alloy grain size, enhancing hardness and wear resistance. Optimal wear resistance was achieved with one ECAE pass, attributed to grain refinement and Mg₂Sn precipitates.
Area of Science:
- Materials Science
- Mechanical Engineering
- Metallurgy
Background:
- Magnesium-tin (Mg-Sn) alloys are crucial for portable electronics and automotive applications due to their lightweight properties.
- Understanding the mechanical behavior of Mg-Sn alloys under processing is vital for optimizing their performance.
Purpose of the Study:
- To characterize the mechanical properties, specifically hardness and wear behavior, of Mg-5wt.% Sn alloy after Equal Channel Angular Extrusion (ECAE).
- To investigate the influence of ECAE processing on the microstructure and its correlation with mechanical performance.
Main Methods:
- Vickers hardness testing and pin-on-disc wear testing were employed to evaluate mechanical properties.
- Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used for microstructural analysis.
- The study involved processing Mg-Sn alloy through multiple passes of ECAE.
Main Results:
- ECAE significantly refined the grain size of Mg-Sn alloy, decreasing it from 117.6 μm (as-cast) to 24.4 μm (four passes).
- Hardness of the alloy improved substantially with ECAE processing.
- Maximum wear resistance of 73.77 m/mm³ was observed after one ECAE pass, linked to grain refinement and Mg₂Sn precipitation.
Conclusions:
- Grain refinement through ECAE enhances the hardness and wear resistance of Mg-Sn alloys.
- While single-pass ECAE improves wear resistance, multi-pass processing can lead to increased oxidative and abrasive wear due to higher internal energy and oxide debris formation.
- The study highlights the trade-offs in optimizing Mg-Sn alloy performance through ECAE, balancing grain refinement benefits against increased oxidation in multi-pass treatments.

