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Updated: Feb 16, 2026

Applying Dynamic Strain on Thin Oxide Films Immobilized on a Pseudoelastic Nickel-Titanium Alloy
Published on: July 28, 2020
Low Environmental Temperature Influences the Fatigue Resistance of Nickel-titanium Files
Ya Shen1, Xiangya Huang2, Zhejun Wang3
1Division of Endodontics, Department of Oral Biological and Medical Sciences, Faculty of Dentistry, Vancouver, British Columbia, Canada; Department of Materials Engineering, The University of British Columbia, Vancouver, British Columbia, Canada.
Introduction:
The purpose of this study was to evaluate the effect of different temperatures (0°C, 10°C, 22°C, 37°C, and 60°C) on the cyclic fatigue life of nickel-titanium (NiTi) files using a new fatigue test model in zirconium oxide.
Methods:
Three superelastic NiTi files (EndoSequence [Brasseler USA, Savannah, GA], ProFile [Dentsply Tulsa Dental Specialties, Tulsa, OK], and K3 [SybronEndo, Orange, CA]), and 3 heat-treated (K3XF [SybronEndo], Vortex [Dentsply Tulsa Dental Specialties], and HyFlex CM [Coltene-Whaledent, Allstetten, Switzerland]) NiTi files, all size 25/.04, were subjected to cyclic fatigue tests inside a novel, artificial ceramic canal with a curvature of 60° and a 5-mm radius. The model was immersed in water at 5 different preset temperatures. The number of cycles to failure (NCF) was recorded, and the fracture surface of the fragments was examined by a scanning electron microscope. The data were analyzed using 2-way analysis of variance with the significance level at 0.05.
Results:
When the temperature was reduced from 60°C to 0°C, the NCF significantly increased from over 2 to 10 times for the NiTi file groups (P < .01). K3XF had the highest fatigue resistance of all files at 0°C (P < .05). Vortex files had the highest NCF at 10°C-60°C. The NCF of heat-treated files was significantly higher than superelastic NiTi files at 10°C and 20°C (P < .05). There was no significant difference in the NCF of HyFlex CM at 0°C and 22°C. There was little difference in the fractographic appearance among different temperatures, except that the fraction area occupied by the dimple region of some instruments at 0°C was slightly smaller than at 60°C.
Conclusions:
Cooling down to low temperatures may be an interesting strategy to improve the fatigue resistance of rotary NiTi files.
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