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Updated: Feb 15, 2026

Characterization of Ultra-fine Grained and Nanocrystalline Materials Using Transmission Kikuchi Diffraction
Published on: April 1, 2017
Influence of grain morphology on ultrasonic wave attenuation in polycrystalline media with statistically equiaxed
Martin Ryzy1, Tomáš Grabec2, Petr Sedlák3
1Research Center for Non-Destructive Testing GmbH, Altenberger Strasse 69, 4040 Linz, Austria.
Abstract:
The influence of a polycrystals' grain structure on elastic wave scattering is studied with analytical and numerical methods in a broad frequency range. A semi-analytical attenuation model, based on an established scattering theory, is presented. This technique accurately accounts for the grain morphology without prior assumptions on grain statistics. This is achieved by incorporating a samples' exact spatial two-point correlation function into the theory. The approach is verified by using a finite element method (FEM) to simulate P-wave propagation in 3D Voronoi crystals with equal mean grain diameter, but different grain shape uniformity. Aluminum and Inconel serve as representatives for weak and strong scattering cubic class materials for simulations and analytical calculations. It was found that the shape of the grains has a strong influence on the attenuation curve progression in the Rayleigh-stochastic transition region, which was attributed to mode conversion scattering. Comparisons between simulations and theory show excellent agreement for both materials. This demonstrates the need for accurately taking the microstructure of heterogeneous materials into account, to get precise analytical predictions for their scattering behaviour. It also demonstrates the impressive accuracy and flexibility of the scattering theory which was used.
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