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Influence of Substrate Moisture State and Roughness on Interface Microstructure and Bond Strength: Slant Shear vs.
Dale P Bentz1, Igor De la Varga2, Jose F Muñoz2
1Engineering Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899.
The optimal substrate moisture for repair material application depends on the testing method. Dry substrates excel in shear tests, while saturated-surface-dry (SSD) substrates perform better in pull-off tests due to microstructural differences.
Area of Science:
- Construction Materials Science
- Civil Engineering
- Materials Science
Background:
- Conflicting literature exists on the ideal substrate moisture state (saturated-surface-dry or dry) for repair material application.
- Testing methodologies, specifically pull-off (direct tension) versus shear, may influence observed bond performance.
- Understanding interfacial microstructure is crucial for optimizing repair material bonding.
Purpose of the Study:
- To investigate the interfacial microstructure developed when repair material is applied to dry versus saturated-surface-dry (SSD) substrates.
- To observe dynamic microstructural rearrangements during the initial curing phase.
- To formulate a hypothesis explaining the influence of substrate moisture on bond test results.
Main Methods:
- Application of various microstructural characterization tools.
- Simultaneous neutron and X-ray radiography to observe dynamic microstructural changes.
- Analysis of water movement and particle densification at the interface during the first 4 hours of curing.
Main Results:
- Differences in water movement and particle densification were observed between dry and SSD substrate specimens.
- Dry substrates showed increased frictional resistance in shear loading due to particle compaction.
- SSD substrates exhibited higher bond strengths in pull-off tests.
Conclusions:
- The optimal substrate moisture state is dependent on the bond testing configuration (shear vs. pull-off) and substrate roughness.
- Particle compaction at dry substrate surfaces enhances shear resistance but offers minimal benefit in pull-off tests.
- Maximizing repair material bond performance requires consideration of material fluidity, substrate roughness, and moisture state.
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