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Updated: Feb 8, 2026

Scalable Syntheses of Graphene Oxide and Reduced Graphene Oxide using Cascade Design Oxidation and Highly Basic Reduction Reactions
Published on: July 3, 2025
In situ atomic-scale observation of inhomogeneous oxide reduction
Xiaobo Chen1, Dongxiang Wu, Lianfeng Zou
1Program of Materials Science and Engineering, Department of Mechanical Engineering, State University of New York at Binghamton, NY 13902, USA. gzhou@binghamton.edu.
Abstract:
We report in situ atomic-scale transmission electron microscopy observations of the surface dynamics during Cu2O reduction. We show inhomogeneous oxide reduction caused by the preferential adsorption of hydrogen at step edges that induces oxygen loss and destabilizes Cu atoms within the step edge, thereby resulting in the retraction motion of atomic steps at the oxide surface.
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