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Area of Science:

  • Synchrotron radiation science
  • Materials characterization
  • X-ray spectroscopy

Background:

  • Remote access is standard for macromolecular crystallography beamlines due to automation.
  • X-ray absorption fine structure (XAFS) beamlines lack widespread remote access capabilities.
  • XAFS experiments present unique challenges due to high variability in experimental conditions.

Purpose of the Study:

  • To describe automation experiences and developments at LNLS and Diamond.
  • To address the challenges hindering remote access for XAFS beamlines.
  • To facilitate broader adoption of remote operation for XAFS experiments.

Main Methods:

  • Review of automation efforts at LNLS (Brazilian Synchrotron Light Laboratory).
  • Review of automation developments at Diamond Light Source.
  • Analysis of specific challenges in XAFS experimental configurations.

Main Results:

  • Detailed account of automation strategies implemented at two major synchrotron facilities.
  • Identification of key factors contributing to the difficulty of automating XAFS beamlines.
  • Insights into potential solutions for overcoming experimental variability.

Conclusions:

  • Automation is crucial for enabling remote access to XAFS beamlines.
  • Further development is needed to standardize and generalize XAFS automation.
  • Successful automation will enhance accessibility and efficiency of XAFS research.