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Predicting lipstick sensory properties with laboratory tests.

D W Rafferty1, L Dupin2, J Zellia1

  • 1Lubrizol Advanced Materials, 9911 Brecksville Rd., Brecksville, OH, 44141, U.S.A.

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Summary

This study aimed to find faster ways to test lipstick properties without relying on human panels. Researchers created twelve lipstick samples with different emollients and tested them using laboratory tools like friction and tack tests. They found that a friction test alone could predict sensory properties like spreadability and stickiness. These results matched what a small panel of people reported. The study shows that physical tests can replace or supplement sensory panels, helping companies develop lipsticks more quickly and affordably.

Keywords:
claim substantiationcolour cosmeticsformulation/stabilitylipstick formulation testingcosmetic sensory evaluationemollient impact on cosmeticstribology in personal care

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Area of Science:

  • Cosmetic formulation science
  • Sensory evaluation in consumer products
  • Materials tribology in personal care

Background:

Developing new lipstick formulations requires evaluating sensory properties like spreadability and gloss. These assessments typically rely on human panels, which are costly and slow. Prior research has shown that physical properties of materials can influence sensory perceptions. However, no prior work had resolved how to predict these perceptions using only laboratory tests. This gap motivated the search for objective methods to assess lipstick properties. Existing studies have linked emollient types to sensory outcomes, but not through predictive models. The need for faster, more affordable testing drove this investigation. Researchers aimed to find correlations between physical measurements and sensory data. They focused on how emollients affect both performance and perception. The goal was to replace or supplement sensory panels with controlled experiments.

Purpose Of The Study:

The study aimed to create laboratory tests that could predict sensory properties of lipsticks without human panels. Specifically, the researchers wanted to test if physical measurements could replace subjective evaluations. They focused on spreadability, stickiness, opacity, and gloss as key attributes. The motivation was to reduce reliance on in vivo testing, which is time-consuming. By varying emollients in formulations, they could isolate sensory effects. The team sought to identify which tests best predicted panel results. They also wanted to determine if a single test could capture multiple attributes. The ultimate goal was to accelerate lipstick development through objective methods.

Main Methods:

The researchers prepared twelve model lipstick formulations with varied emollients. Each formulation had distinct sensory and performance properties. A nine-person panel evaluated spreadability, stickiness, opacity, and gloss. For performance testing, a CETR UMT-2 tribometer measured friction. An analytical balance assessed application properties. A Texture Analyser TA.XT-Plus tested tack. Photography and image analysis evaluated colour development and retention. The data from these tests were statistically compared to panel results. The goal was to find correlations between physical measurements and sensory perceptions.

Main Results:

Laboratory tests correlated strongly with sensory panel results. Friction tests grouped lipsticks into oily, creamy, waxy, and sticky categories. These classifications matched data from other performance tests. Surprisingly, friction tests alone predicted all four sensory attributes. The coefficient of friction correlated with adhesive and cohesive properties. Emollients influenced these properties, affecting film formation. Statistical models showed high accuracy in predicting panel responses. The friction test proved sufficient for predicting spreadability, stickiness, opacity, and gloss.

Conclusions:

The authors found that friction tests alone could predict key sensory properties. This suggests that physical measurements can replace sensory panels in some cases. The balance of adhesive and cohesive forces explained correlations. Emollients significantly affected both sensory and performance properties. The methods developed may streamline lipstick formulation processes. The study supports using laboratory tests to optimize formulations faster. The results highlight the importance of emollient choice in lipstick design. These findings may help reduce reliance on costly human testing.

Friction tests measure the coefficient of friction, which correlates with adhesive and cohesive forces. These forces influence spreadability, stickiness, opacity, and gloss.

Emollients affect the adhesive and cohesive properties of the lipstick film. Different emollients lead to distinct sensory and performance outcomes.

Friction data captured the balance of adhesive and cohesive forces, which underlie multiple sensory properties like spreadability and stickiness.

The classifications—oily, creamy, waxy, and sticky—reflect distinct physical properties observed in friction and other tests, aligning with sensory perceptions.

The models predicted sensory panel results with high accuracy, showing strong correlations between physical measurements and perceived attributes.

The authors suggest that friction tests alone may replace or supplement sensory panels, accelerating lipstick development and reducing testing costs.