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Facile Analytical Methods to Determine the Purity of Titanium Tetrachloride
Dongwook Lim1, Sang-Deuk Kim1, Hyungseok Kong1
1Department of Chemistry and Chemical Engineering, Center for Design and Applications of Molecular Catalysts, Inha University, Incheon 402-751, Republic of Korea.
Abstract:
We propose a simple method to investigate both the qualitative and quantitative properties of titanium tetrachloride. The selection and concentration of the employed solvent were found to be very important in the analysis of highly reactive titanium tetrachloride (TiCl4). Herein, we employed various concentrations of an acid solution to serve as a stabilizing medium. Qualitative analysis was performed via Fourier transform-infrared spectroscopy (FT-IR) and scanning electron microscope-energy dispersive spectroscopy (SEM-EDS). Additionally, the quantitative analysis was performed via inductively coupled plasma optical emission spectroscopy (ICP-OES). We concluded that both the qualitative and quantitative properties of titanium tetrachloride could be easily measured using a specific acidic solvent as a medium.
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