An ultra-compact low temperature scanning probe microscope for magnetic fields above 30 T.
L Rossi1, J W Gerritsen2, L Nelemans1
1High Field Magnet Laboratory (HFML-EMFL), Radboud University, Nijmegen, The Netherlands.
The Review of Scientific Instruments
|December 4, 2018
Summary
We developed a compact high field scanning probe microscope (HF-SPM) for extreme 38 T magnetic fields. This instrument enables topographic imaging and magnetostriction measurements at cryogenic temperatures.
Area of Science:
- Condensed Matter Physics
- Materials Science
- Nanotechnology
Background:
- Scanning probe microscopy (SPM) is crucial for nanoscale characterization.
- Operating SPM in extreme environments like high magnetic fields presents significant challenges.
- Previous SPM systems were limited in their ability to function under such conditions.
Purpose of the Study:
- To design and demonstrate a highly compact high field scanning probe microscope (HF-SPM).
- To enable SPM operation at cryogenic temperatures within extremely high magnetic fields (up to 38 T).
- To characterize and mitigate vibrational noise from a Bitter magnet for reliable SPM measurements.
Main Methods:
- Development of a 14 mm diameter HF-SPM incorporating an Attocube nano-positioner.
- Utilizing a water-cooled Bitter magnet capable of generating fields up to 38 T.
- Characterization of Bitter magnet-induced vibrational noise up to 300 kHz and implementation of noise mitigation strategies.
- Performance validation through topographic imaging and noise measurements up to 30 T.
Main Results:
- Successful design and implementation of a compact HF-SPM.
- Demonstrated topographic imaging and noise measurements at magnetic fields up to 30 T.
- Characterization of vibrational noise and successful mitigation techniques.
- Validation of the HF-SPM as a 3D dilatometer for magnetostriction measurements on a spinel sample.
Conclusions:
- The developed HF-SPM is a viable tool for nanoscale investigation in ultra-high magnetic fields.
- The system overcomes the challenges posed by extreme magnetic environments for SPM.
- The HF-SPM opens new avenues for studying material properties under extreme conditions, including magnetostriction.
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