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N,N-Dimethylformamide (DMF) Usage in Epoxy/Graphene Nanocomposites: Problems Associated with Reaggregation
Jiacheng Wei1, Mohd Shahneel Saharudin2, Thuc Vo3
1Faculty of Engineering and Environment, Department of Mechanical and Construction Engineering, Northumbria University, Newcastle upon Tyne NE1 8ST, UK. jiacheng.wei@northumbria.ac.uk.
Polymers
|April 12, 2019
Summary
Dimethylformamide (DMF) dosage impacts epoxy/graphene nanocomposite properties. Excessive DMF can hinder graphene dispersion, leading to reaggregation and suboptimal material characteristics.
Area of Science:
- Materials Science
- Polymer Chemistry
- Nanotechnology
Background:
- Dimethylformamide (DMF) is a common solvent for creating graphene nanocomposites.
- Existing research focuses on property improvements, neglecting DMF's processing influence.
Purpose of the Study:
- To investigate how varying dimethylformamide (DMF) dosages affect the processing and final properties of epoxy/graphene nanocomposites.
- To understand the relationship between DMF concentration and graphene dispersion.
Main Methods:
- Preparation of epoxy/graphene nanocomposites using different DMF dosages.
- Analysis using mechanical testing, X-ray diffraction (XRD), dynamic mechanical analysis (DMA), thermogravimetric analysis (TGA), and scanning electron microscopy (SEM).
Main Results:
- DMF dosage significantly influences the dispersion and properties of graphene within the epoxy matrix.
- Higher DMF concentrations can lead to graphene reaggregation, negatively impacting nanocomposite quality.
- Optimal DMF dosage is crucial for achieving desired material properties.
Conclusions:
- The effectiveness of DMF in preparing epoxy/graphene nanocomposites is dosage-dependent.
- Excessive DMF is detrimental to graphene dispersion and overall nanocomposite performance.
- Further research should optimize DMF usage for superior nanocomposite fabrication.
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