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Acridine form IX
Peter W Stephens1, Einat Schur2, Saul H Lapidus1,3
1Department of Physics and Astronomy, Stony Brook, NY 11794-3800, USA.
Abstract:
We report a new polymorph of acridine, C13H9N, denoted form IX, obtained as thin needles by slow evaporation of a toluene solution. The structure was solved and refined from powder X-ray data. The structures of five unsolvated forms were previously known, but this is only the second with one mol-ecule in the asymmetric unit. The melting point [differential scanning calorimetry (DSC) onset] and heat of fusion are 108.8 (3) °C and 19.2 (4) kJ mol-1, respectively.
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