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Updated: Jan 22, 2026

Preparation of Fungal and Plant Materials for Structural Elucidation Using Dynamic Nuclear Polarization Solid-State NMR
Published on: February 12, 2019
Large volume liquid state scalar Overhauser dynamic nuclear polarization at high magnetic field
Thierry Dubroca1, Sungsool Wi, Johan van Tol
1NHMFL, 1800 E. Paul Dirac Dr, Tallahassee, FL 32310, USA. dubroca@magnet.fsu.edu.
Abstract:
Dynamic Nuclear Polarization (DNP) can increase the sensitivity of Nuclear Magnetic Resonance (NMR), but it is challenging in the liquid state at high magnetic fields. In this study we demonstrate significant enhancements of NMR signals (up to 70 on 13C) in the liquid state by scalar Overhauser DNP at 14.1 T, with high resolution (∼0.1 ppm) and relatively large sample volume (∼100 μL).
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