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Updated: Jan 21, 2026

Characterization of Ultra-fine Grained and Nanocrystalline Materials Using Transmission Kikuchi Diffraction
Published on: April 1, 2017
Achieving excellent microformability in aluminum by engineering a unique ultrafine-grained microstructure.
A Dhal1, S K Panigrahi2, M S Shunmugam1
1Manufacturing Engineering Section, Department of Mechanical Engineering, Indian Institute of Technology Madras, Chennai, 600036, India.
Engineering ultrafine-grained (UFG) materials with equiaxed grains significantly enhances microformability by enabling grain boundary-mediated plasticity. This microstructure overcomes limitations seen in other UFG and conventional materials during microforming processes.
Area of Science:
- Materials Science
- Mechanical Engineering
- Nanotechnology
Background:
- Microforming conventional materials faces challenges due to the proximity of specimen and microstructural length-scales, leading to abnormal deformation and reduced microformability.
- Engineering ultrafine-grained (UFG) microstructures is a potential solution, but their micro-scale deformation behavior requires comprehensive understanding.
Purpose of the Study:
- To investigate the micro-scale deformation behavior of four distinct microstructures: UFG with residual dislocations/elongated grains, UFG with equiaxed grains, bimodal-grained, and coarse-grained materials.
- To identify the microstructural characteristics responsible for enhanced microformability.
Main Methods:
- Micro-scale uniaxial tensile testing.
- Micro-deep drawing operations.
- Postmortem microscopy analysis of formed micro-parts.
Main Results:
- Micro-cups formed from UFG material with equiaxed grains exhibited superior surface quality, form accuracy, and minimal process variation.
- Improved microformability in equiaxed UFG material is attributed to grain boundary-mediated plasticity, including synergistic grain migration and rotation.
- Residual dislocations, elongated grains, and coarser microstructures (bimodal, coarse-grained) led to strain localization, thinning, and reduced microformability due to hindered grain movement or dominance of cross-slip.
Conclusions:
- Equiaxed ultrafine-grained microstructures offer superior microformability due to effective grain boundary-mediated plasticity mechanisms.
- Material microstructure engineering is critical for optimizing performance in microforming applications.
- Understanding deformation mechanisms at the micro-scale is essential for advancing micro-manufacturing technologies.
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