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Published on: April 11, 2021
In-situ Electrochemical X-ray Diffraction: A Rigorous Method to Navigate within Phase Diagrams Reveals β-Fe1+x Se as
Bertold Rasche1, Minjun Yang1, Lothar Nikonow1
1Department of Chemistry, University of Oxford, Oxford, OX1 3QZ, UK.
Abstract:
We report the precise postsynthetic control of the composition of β-Fe1+x Se by electrochemistry with simultaneous tracking of the associated structural changes via in situ synchrotron X-ray diffraction. We access the full phase width of 0.01
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