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Evaluation of the Curing of Adhesive Systems by Rheological and Thermal Testing
Published on: July 3, 2020
Can universal adhesive systems bond to zirconia?
Ricardo Alves Dos Santos1, Eliane Alves de Lima1, Luciana Sarmento Mendonça1
1Faculty of Dentistry of Pernambuco, Universidade de Pernambuco - UPE, Camaragibe, Pernambuco, Brazil.
This study investigated whether universal adhesive systems can effectively bond to zirconia, a common dental ceramic. Researchers prepared zirconia blocks and treated them with either polishing or grit-blasting. They then applied different adhesives and tested bond strength. Results showed that grit-blasting significantly improved bond strength compared to polishing. SEM images revealed that grit-blasted surfaces allowed for better mechanical interlocking with adhesives. Universal adhesives performed similarly to conventional ones when used on grit-blasted surfaces. The study suggests that grit-blasting is a practical method to enhance adhesion, and universal adhesives can simplify bonding procedures for zirconia restorations.
Area of Science:
- Dental materials science
- Restorative dentistry
- Adhesive bonding techniques
Background:
Zirconia is a widely used ceramic material in dental restorations due to its strength and aesthetics. However, achieving durable bonding to zirconia remains a challenge. Traditional bonding methods often require specific surface treatments to enhance adhesion. Prior research has shown that grit-blasting with alumina particles can increase surface roughness and improve bond strength. Yet, the effectiveness of universal adhesive systems on zirconia surfaces remains unclear. This gap motivated a study to evaluate whether these systems can bond effectively to zirconia. No prior work had resolved the compatibility of universal adhesives with zirconia under various surface treatments. Understanding this could influence clinical protocols for bonding and repairing zirconia-based restorations. The study aimed to compare bond strength outcomes using different adhesives and surface treatments. This knowledge is essential for optimizing dental restoration techniques involving zirconia.
Purpose Of The Study:
The study aimed to evaluate the bond strength of universal adhesive systems to zirconia under two surface treatments. The specific problem addressed was whether these systems could reliably bond to zirconia without requiring specialized protocols. The motivation stemmed from the need to simplify clinical bonding procedures for zirconia restorations. Zirconia’s inert surface makes bonding difficult, prompting the need for effective adhesives. The study focused on comparing polished and grit-blasted zirconia surfaces. It also tested combinations of adhesives to determine if any provided superior results. The goal was to assess whether universal adhesives could replace conventional methods. This could impact clinical practices by reducing the need for multiple bonding agents.
Main Methods:
Eighty zirconia blocks were prepared using CAD/CAM milling and embedded in PVC tubes. The blocks were polished or grit-blasted with alumina particles to create two surface treatment groups. Each group was further divided into four subgroups based on the adhesive used: Z-Prime Plus (control), Scotchbond Universal, All Bond Universal, and a combination of Z-Prime Plus and All Bond Universal. Composite resin was applied to the blocks using a two-part metal die. Specimens were stored for 24 hours before undergoing microshear bond strength testing. Statistical analysis included ANOVA, Student’s t-test, and Tukey’s test to compare results. Scanning electron microscopy (SEM) was used to examine zirconia surfaces and adhesive interfaces after sputter coating. The methods ensured a controlled comparison of adhesion outcomes across different conditions.
Main Results:
Grit-blasted zirconia showed significantly higher bond strength compared to polished surfaces. No significant differences were observed between adhesive systems in the grit-blasted group. The control adhesive (Z-Prime Plus) performed similarly to universal adhesives in this group. SEM analysis revealed micromechanical retention features on grit-blasted surfaces. Adhesive interfaces exhibited zirconia-adhesive interlocking in blasted specimens. Polished surfaces showed lower bond strength regardless of adhesive used. The combination of Z-Prime Plus and All Bond Universal did not improve outcomes over single adhesives. These findings suggest that grit-blasting is more effective than polishing for enhancing adhesion to zirconia.
Conclusions:
The study found that universal adhesive systems can bond to zirconia, particularly when surfaces are grit-blasted. The authors propose that grit-blasting enhances bond strength through micromechanical retention. No significant differences were observed between universal adhesives in the grit-blasted group. The authors suggest that these systems simplify bonding procedures for zirconia restorations. The findings imply that intraoral repair of zirconia fractures is feasible using universal adhesives. The study supports the clinical use of grit-blasting as a preferred surface treatment. The authors state that universal adhesives offer a practical alternative to conventional bonding agents. These conclusions are based on the observed bond strength and SEM analysis results.
Frequently Asked Questions
The authors propose that grit-blasting creates micromechanical retention and interlocking at the adhesive interface, enhancing bond strength.
The study tested Z-Prime Plus (control), Scotchbond Universal, All Bond Universal, and a combination of Z-Prime Plus and All Bond Universal.
Grit-blasting with alumina particles increases surface roughness, which the authors suggest improves adhesion through micromechanical retention.
SEM analysis revealed micromechanical retention features and interlocking at adhesive interfaces, supporting the observed bond strength differences.
Polished zirconia showed lower bond strength compared to grit-blasted surfaces, regardless of the adhesive used.
The authors propose that universal adhesives simplify bonding to zirconia and enable intraoral repair of fractures when used with grit-blasting.
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