Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Concept Videos

Single Crystal and Powder X-ray Diffraction08:14

Single Crystal and Powder X-ray Diffraction

108.4K
Source: Tamara M. Powers, Department of Chemistry, Texas A&M University 
X-ray crystallography is a technique that uses X-rays to study the structure of molecules. X-ray diffraction (XRD) experiments are routinely carried out with either single-crystal or powdered samples.
Single-crystal XRD:
Single-crystal XRD allows for absolute structure determination. With single-crystal XRD data, the exact atomic positions can be observed, and thus bond lengths and angles can be determined. This...
108.4K
Growing Crystals for X-ray Diffraction Analysis08:00

Growing Crystals for X-ray Diffraction Analysis

33.5K
Source: Laboratory of Dr. Jimmy Franco - Merrimack College
X-ray crystallography is a method commonly used to determine the spatial arrangement of atoms in a crystalline solid, which allows for the determination of the three-dimensional shape of a molecule or complex. Determining the three-dimensional structure of a compound is of particular importance, since a compound's structure and function are intimately related. Information about a compound's structure is often used to explain its...
33.5K
X-ray Diffraction09:31

X-ray Diffraction

92.9K
Source: Faisal Alamgir, School of Materials Science and Engineering, Georgia Institute of Technology, Atlanta, GA
X-ray diffraction (XRD) is a technique used in materials science for determining the atomic and molecular structure of a material. This is done by irradiating a sample of the material with incident X-rays and then measuring the intensities and scattering angles of the X-rays that are scattered by the material. The intensity of the scattered X-rays are plotted as a function of the...
92.9K
High Pressure Single Crystal Diffraction at PX^211:32

High Pressure Single Crystal Diffraction at PX^2

22.1K
In this report, we describe detailed procedures for carrying out single crystal X-ray diffraction experiments with a diamond anvil cell at the GSECARS 13-BM-C beamline at the Advanced Photon Source. ATREX and RSV programs are used to analyze the...
22.1K
Crystallization of Proteins on Chip by Microdialysis for In Situ X-ray Diffraction Studies12:38

Crystallization of Proteins on Chip by Microdialysis for In Situ X-ray Diffraction Studies

7.0K
This paper details the fabrication protocol of microfluidic chips developed for on-chip protein crystallization with the dialysis method and in situ X-ray diffraction experiments. The microfabrication process makes it possible to integrate a semipermeable regenerated cellulose dialysis membrane with any molecular weight cut-off, between two layers of the...
7.0K
On-Chip Crystallization and Large-Scale Serial Diffraction at Room Temperature07:42

On-Chip Crystallization and Large-Scale Serial Diffraction at Room Temperature

2.3K
This contribution describes how to set up protein crystallization on crystal-on-crystal devices and how to perform automated serial data collection at room temperature using the on-chip crystallization...
2.3K

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same authorSame journal

Origin and application of the Lorentz factor in X-ray diffraction.

Acta crystallographica. Section A, Foundations and advances·2026
Same author

Quantitative analysis of light-induced ion segregation in mixed-halide perovskites.

Journal of applied crystallography·2026
Same author

Multi-peak single object emission of MAPbBr<sub>3</sub> nanoplatelets synthesised using a non-template ligand-assisted reprecipitation route.

Nanoscale·2026
Same author

Graphene-Based Nanostructures Produced by Laser Ablation Assisted by Electric Field.

Nanomaterials (Basel, Switzerland)·2026
Same author

Crack-Mitigating Strategy in Directed Energy Deposition of Refractory Complex Concentrated CrNbTiZr Alloy.

Materials (Basel, Switzerland)·2025
Same author

The Structure and Mechanical Properties of FeAlCrNiV Eutectic Complex Concentrated Alloy.

Materials (Basel, Switzerland)·2025

Related Experiment Video

Updated: Jan 20, 2026

Single Crystal and Powder X-ray Diffraction
08:14

Single Crystal and Powder X-ray Diffraction

Published on: April 30, 2023

108.4K

Anomalous X-ray diffraction from ω nanoparticles in β-Ti(Mo) single crystals.

Jana Šmilauerová1, Petr Harcuba1, Miroslav Cieslar1

  • 1Faculty of Mathematics and Physics, Charles University, Ke Karlovu 5, 121 16 Prague, Czech Republic.

Acta Crystallographica. Section A, Foundations and Advances
|September 3, 2019
PubMed
Summary

Anomalous X-ray diffraction reveals molybdenum distribution in Ti-15Mo alloy. Molybdenum is rejected from omega particles, forming a surrounding cloud and causing matrix deformation.

Keywords:
anomalous X-ray diffractiondiffuse scatteringmetastable β-Ti alloysω phase

More Related Videos

Growing Crystals for X-ray Diffraction Analysis
08:00

Growing Crystals for X-ray Diffraction Analysis

Published on: April 30, 2023

33.5K
High Pressure Single Crystal Diffraction at PX^2
11:32

High Pressure Single Crystal Diffraction at PX^2

Published on: January 16, 2017

22.1K

Related Experiment Videos

Last Updated: Jan 20, 2026

Single Crystal and Powder X-ray Diffraction
08:14

Single Crystal and Powder X-ray Diffraction

Published on: April 30, 2023

108.4K
Growing Crystals for X-ray Diffraction Analysis
08:00

Growing Crystals for X-ray Diffraction Analysis

Published on: April 30, 2023

33.5K
High Pressure Single Crystal Diffraction at PX^2
11:32

High Pressure Single Crystal Diffraction at PX^2

Published on: January 16, 2017

22.1K

Area of Science:

  • Materials Science
  • Solid State Physics
  • Crystallography

Background:

  • Metastable beta titanium alloys are crucial engineering materials.
  • Omega (ω) particles influence the mechanical properties of titanium alloys.
  • Understanding solute distribution, like molybdenum (Mo), is key to alloy performance.

Purpose of the Study:

  • To investigate the spatial distribution of molybdenum (Mo) in a Ti-15Mo alloy.
  • To analyze the influence of ω particles on Mo distribution using Anomalous X-ray Diffraction (AXRD).
  • To characterize the diffuse scattering patterns and their energy dependence near the Mo K absorption edge.

Main Methods:

  • Anomalous X-ray Diffraction (AXRD) experiments were conducted around the Mo K edge (20.0 keV).
  • Diffuse scattering patterns near the (006)β diffraction maximum were analyzed.
  • Numerical simulations of diffuse scattering and energy dependencies were performed.

Main Results:

  • Observed variations in diffracted intensity with incident photon energy near the absorption edge.
  • Confirmed Mo rejection from ω particles during their growth.
  • Identified elastic deformation of the β matrix due to ω particles and a surrounding Mo-rich cloud.

Conclusions:

  • AXRD is effective for mapping solute distribution in alloys.
  • The presence of ω particles induces local matrix strain and Mo segregation.
  • The findings provide insights into the phase evolution and mechanical behavior of Ti-15Mo alloys.