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Updated: Jan 20, 2026

Supercritical Nitrogen Processing for the Purification of Reactive Porous Materials
Published on: May 15, 2015
Porous materials of nitrogen doped graphene oxide@SnO2 electrode for capable supercapacitor application
Sivalingam Ramesh1, H M Yadav2, Young-Jun Lee3
1Department of Mechanical, Robotics and Energy Engineering, Dongguk University-Seoul, Pil-dong, Jung-gu, 04620, Seoul, Republic of Korea.
Tin oxide@nitrogen-doped graphene oxide (SnO2@NGO) composites were synthesized for high-performance supercapacitors. These materials demonstrate excellent specific capacitance and cycle stability, showing promise for energy storage applications.
Area of Science:
- Materials Science
- Electrochemistry
- Nanotechnology
Background:
- Supercapacitors require advanced electrode materials for enhanced energy storage.
- Nanostructured metal oxides combined with carbon materials offer synergistic benefits.
Purpose of the Study:
- To synthesize and characterize porous SnO2@NGO composites.
- To evaluate the electrochemical performance of SnO2@NGO for supercapacitor applications.
Main Methods:
- Thermal reduction synthesis at 550°C using ammonia and urea.
- Characterization using Raman, XRD, XPS, HR-TEM, FE-TEM, and BET analysis.
- Electrochemical testing including cyclic voltammetry (CV), galvanostatic charge-discharge (GCD), and electrochemical impedance spectroscopy (EIS).
Main Results:
- Successful synthesis of SnO2 nanoparticles anchored on NGO composite at the nanoscale.
- Achieved specific capacitance of ~378 F/g at 4 A/g.
- Demonstrated excellent cycle stability up to 5000 cycles.
Conclusions:
- The synthesized SnO2@NGO composite exhibits promising electrochemical properties.
- This material is a strong candidate for high-performance supercapacitor applications.
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