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Updated: Jan 19, 2026

Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques
Published on: November 11, 2013
Structural and morphological dataset for rf-sputtered WC-Co thin films using synchrotron radiation methods
R R Phiri1, O P Oladijo1,2, H Nakajima3
1Department of Chemical, Materials and Metallurgical Engineering, Botswana International University of Science and Technology, Private Bag 16, Palapye, Botswana.
Abstract:
Control and manipulation of synthesis parameters of thin film coatings is of critical concern in determination of material properties and performance. Structural and morphological properties of rf-sputtered WC-Co thin films deposited under varying deposition parameters namely, substrate temperature and rf power are presented in this data article. The surface morphology, crystallite size and nature were acquired using x-ray photoelectron spectroscopy (XPS) and Grazing Incidence X-ray absorption spectroscopy (GI-XAS). Furthermore, Synchrotron findings are correlated with complimentary data acquired from Scanning electron microscopy (SEM), Raman spectroscopy and surface profilometry to predict and point out optimum synthesis parameters for best properties of the film.
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